Method for quantitatively characterizing pores in shale

A quantitative characterization, pore technology, applied in measurement devices, permeability/surface area analysis, suspension and porous material analysis, etc., can solve the problems of not really revealing the actual size of shale pores, expensive, and difficult to operate.

Active Publication Date: 2018-12-07
HUNAN UNIV OF SCI & TECH +1
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Problems solved by technology

Conventional physical property testing, for shale, it is difficult to obtain the column used for analysis (because shale is fragile); and the current popular mercury injection, CO 2 or N 2 Adsorption only reflects the size of shale pores from the aspects of specific surface area and specific surface volume, but does not really reveal the actual size of shale pores; although CT analysis technology can fully reveal the size of micro-nano pores in shale, the price expensive, not easy to operate

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  • Method for quantitatively characterizing pores in shale
  • Method for quantitatively characterizing pores in shale
  • Method for quantitatively characterizing pores in shale

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Embodiment Construction

[0035] The present invention will be described in further detail below.

[0036] A method for quantitative characterization of pores in shale, comprising the steps of:

[0037] S1: Sample pretreatment and optical film preparation: For the collected shale samples, inject epoxy resin under high-pressure vacuum state, pay attention to control the pressure during injection to ensure that the shale samples are destroyed, and then inject epoxy resin The shale sample is ground into a laser confocal optical sheet, which requires an optical sheet size of about 1mm in thickness, or even thinner, with an area of ​​3×2cm or 3×3cm;

[0038] S2: Two-dimensional laser slice scanning and identification of pores in shale: 2D laser scanning was performed on the confocal laser slice prepared in S1 with a step size of 1.33 um and a resolution of 400 Hz to obtain a series of 2D Laser sectioning (that is, two-dimensional laser confocal micrographs); secondly, since the pores in shale are mainly comp...

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Abstract

The invention relates to a method for quantitatively characterizing pores in shale. The method comprises the following steps: S1, collecting a shale sample and injecting epoxy resin into the collectedshale sample in a high-temperature and high-pressure state; then grinding the shale sample with the injected epoxy resin into a laser confocal optical sheet; S2, carrying out optical slicing on the laser confocal optical sheet prepared by S1 in a laser scanning mode, so as to obtain a series of two-dimensional laser confocal photomicrographs; S3, based on identification of pores in the shale in S2, classifying the pores in the identified shale; and S4, carrying out three-dimensional modeling and quantitative characterization on the pores in the shale by applying three-dimensional modeling software. According to the method provided by the invention, the pores with different formation factors in the shale are identified by applying a fluorescent technology, and different pore types in the shale are divided; and a two-dimensional fluorescent confocal slice is subjected to three-dimensional fluorescent modeling and quantitative characterization of the pores in the shale.

Description

technical field [0001] The invention relates to a quantitative calculation method for pores in continental shale, in particular to a quantitative characterization method for pores in shale. Background technique [0002] With the large-scale exploration and development of shale oil and gas in China, China's continental shale has once again become the focus of global attention. For China, in the exploration of conventional oil and gas resources, the reservoir is already very tight, and has already entered the era of low porosity and low permeability, even ultra-low porosity and ultra-low permeability. For example, the Paleozoic natural gas reservoirs in the Ordos Basin have reached the level of low porosity and low permeability to ultra-low porosity and low permeability. For mud shale in continental deposits, the reservoir appears to be tighter. As we all know, for shale oil and gas, the identification and quantification of micro-nano pores in shale, and the classification o...

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Application Information

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IPC IPC(8): G01N15/08
CPCG01N15/088
Inventor 黄俨然谭静强黄军平肖正辉余烨
Owner HUNAN UNIV OF SCI & TECH
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