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Preparation method and application in cigarettes of cigarette momordica grosvenori perfume

A technology of Luo Han Guo and spices, which is applied in the field of preparation of Luo Han Guo spices for cigarettes, to achieve the effects of increasing sweetness, comfortable aftertaste, and reducing irritation and miscellaneous gas

Inactive Publication Date: 2018-11-23
CHINA TOBACCO GUANGXI IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there is no use of membrane separation technology to separate the Luo Han Guo extract to prepare tobacco flavors

Method used

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  • Preparation method and application in cigarettes of cigarette momordica grosvenori perfume

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Take the dried Luo Han Guo medicinal material, pulverize it into a coarse powder, and pass it through a 10-mesh stainless steel screen; accurately weigh the Luo Han Guo powder, place it in a percolation cylinder, add 11 times the amount of 65% ethanol, soak it for 24 hours after wetting; at 5mL / min Speed ​​percolation extraction, until the percolation liquid with a mass of 10 times the mass of the coarse powder of medicinal materials is obtained, the extraction is terminated, and the percolation liquid is filtered for later use; the percolation hydraulic distillation is taken until no ethanol flows out, and the Luo Han Guo extract is obtained.

[0030] Accurately weigh the Luo Han Guo extract and place it in a quantitative glass container, add 50 times the amount of 20% ethanol to dissolve, and the dissolved solution is D1. After the dissolution is complete, use a 50nm ceramic microfiltration membrane to filter, and the cut-off section is D2; the permeate liquid of the m...

Embodiment 2

[0033] Take the dried Luo Han Guo medicinal material, pulverize it into a coarse powder, and pass it through a 10-mesh stainless steel screen; accurately weigh the Luo Han Guo powder, place it in a percolation cylinder, add 20 times the amount of 50% ethanol, soak it for 24 hours after wetting; use 2 mL / min Speed ​​percolation extraction, until the percolation liquid with a mass of 18 times the mass of the coarse powder of medicinal materials is obtained, the extraction is terminated, and the percolation liquid is filtered for later use; the percolation liquid is hydraulically distilled until no ethanol flows out, and the Luo Han Guo extract is obtained.

[0034] Accurately weigh the Luo Han Guo extract and place it in a quantitative glass container, add 50 times the amount of 20% ethanol to dissolve, and the dissolved solution is D1. After the dissolution is complete, use a 200nm ceramic microfiltration membrane to filter, and the cut-off section is D2; the permeate liquid of ...

Embodiment 3

[0037] Take the dried Luo Han Guo medicinal material, pulverize it into a coarse powder, and pass it through a 10-mesh stainless steel screen; accurately weigh the Luo Han Guo powder, place it in a percolation cylinder, add 5 times the amount of 95% ethanol, soak it for 24 hours after wetting; at 10mL / min Speed ​​percolation extraction, until the percolation liquid with a mass of 4 times the mass of the coarse powder of medicinal materials is obtained, the extraction is terminated, and the percolation liquid is filtered for later use; the percolation liquid is hydraulically distilled until no ethanol flows out, and the Luo Han Guo extract is obtained.

[0038] Accurately weigh the Luo Han Guo extract and place it in a quantitative glass container, add 50 times the amount of 20% ethanol to dissolve, and the dissolved solution is D1. After the dissolution is complete, use a 100nm ceramic microfiltration membrane to filter, and the cut-off section is D2; the permeate liquid of the...

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Abstract

The invention provides a preparation method of cigarette momordica grosvenori perfume. The method comprises the steps that fresh and ripe momordica grosvenori is pulverized and screened, ethanol soaking is conducted for 24 hours, percolation extraction is conducted in a certain flow rate to obtain a certain amount of percolation extract, and filtering and concentrating are conducted to obtain momordica grosvenori extract; ethanol dissolving is conducted on the momordica grosvenori extract, large molecular substances are removed by filtering using a ceramic microfiltration membrane, microfiltration membrane permeation liquid is filtered through an organic ultrafiltration membrane to remove part of small molecular substances influencing fragrance and taste, part of the organic ultrafiltration membrane is reserved, and pressure reduction, distillation and concentration are conducted to obtain the momordica grosvenori perfume. The invention further discloses the application of the perfumein cigarettes, the cigarette momordica grosvenori perfume is diluted and sprayed on cut tobacco in a certain ratio, and the cut tobacco is rolled and produced into cigarettes. After adding the perfume, the fragrance diversity can be obviously increased, the smoothness of smoking fume is increased, sweet taste is increased, irritation and impurity gas can be reduced, therefore the smoking fume is gentle, and remaining smell is comfortable.

Description

Technical field: [0001] The invention belongs to the technical field of preparation of tobacco additives, and in particular relates to a preparation method of monk fruit fragrance for tobacco and its application in cigarettes. technical background: [0002] Luo Han Guo, the fruit of perennial vines of Cucurbitaceae. Also known as Lahan Guo, False Bitter Gourd, Light Fruit Wood Softshell Turtle, Jinbuhuan, Luohanbiao, Naked Turtle, it is known as the "fairy fruit". Its leaves are heart-shaped, dioecious, blooming in summer and fruiting in autumn. It is mainly produced in Yongfu County and Longsheng County, Guilin City, Guangxi Zhuang Autonomous Region. Yongfu County and Longsheng County are the hometowns of Luo Han Guo with a long history of cultivation. Among them, Yongfu has a history of planting Luo Han Guo for more than 300 years, and Longsheng County has a history of planting Luo Han Guo for more than 200 years. Ninety percent of Luo Han Guo is produced in Yongfu County...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24B3/12A24B15/24C11B9/02
CPCA24B3/12A24B15/241C11B9/022C11B9/025C11B9/027
Inventor 吴彦黄东业胡志忠宁振兴农李政刘鸿李志华徐石磊杨龙彦廖超执宋凌勇陈义昌黄善松胡超班强务文涛薛云
Owner CHINA TOBACCO GUANGXI IND
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