Preparation method for indium trisulfide@graphene oxide nanocomposite
A nanocomposite material, indium trisulfide technology, is applied in chemical instruments and methods, physical/chemical process catalysts, chemical/physical processes, etc., to achieve the effects of reducing production costs, low energy consumption, and excellent synergistic catalysis effect.
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Embodiment 1
[0023] Dissolve 1 gram of indium trisulfide in 1 liter of ethanol, add 10 milliliters of KH550, and stir for 11 hours to obtain a solid-liquid mixture. Wash twice with 100 ml of distilled water and 100 ml of absolute ethanol in turn. The solid is taken out with ethanol and dried in vacuum at 60 degrees Celsius for 2 hours at a vacuum degree of 0.09. Dissolve 0.05 g of graphene oxide in distilled water, add the solid obtained after sensitization, and stir for 12 hours to obtain a solid-liquid mixture. Wash twice with 100 ml of distilled water and 100 ml of absolute ethanol in turn. The solid is taken out with ethanol and dried in vacuum at 50°C for 2 hours.
Embodiment 2
[0025] Dissolve 1.2 g of indium trisulfide in 1 liter of ethanol, add 12 ml of KH550, and stir for 11 hours and 30 minutes to obtain a solid-liquid mixture. Wash twice with 100 ml of distilled water and 100 ml of absolute ethanol in turn. The solid is taken out with ethanol and dried in vacuum at 60 degrees Celsius for 2 hours at a vacuum degree of 0.09. Dissolve 0.07 g of graphene oxide in distilled water, add the solid obtained after sensitization, and stir for 12 hours to obtain a solid-liquid mixture. Wash twice with 100 ml of distilled water and 100 ml of absolute ethanol in turn. The solid is taken out with ethanol and dried in vacuum at 50°C for 2 hours.
Embodiment 3
[0027] Dissolve 1.4 g of indium trisulfide in 1 liter of ethanol, add 14 ml of KH550, and stir for 12 hours to obtain a solid-liquid mixture. Wash twice with 100 ml of distilled water and 100 ml of absolute ethanol in turn. The solid is taken out with ethanol and dried in vacuum at 60 degrees Celsius for 2 hours at a vacuum degree of 0.09. Dissolve graphene oxide in distilled water, add the solid obtained after sensitization, and stir for 12 hours to obtain a solid-liquid mixture. Wash twice with 100 ml of distilled water and 100 ml of absolute ethanol in turn. The solid is taken out with ethanol and dried in vacuum at 50°C for 2 hours.
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