C55E spring steel spheroidizing annealing etchant solution and preparation method and application method of solution
A corrosion solution and annealing technology, which is applied in the field of C55E spring steel spheroidizing annealing corrosion solution, can solve the problems of corrosion of C55E carbon spring steel, obstruction, and inability to obtain quantitative data of grain size, etc., and achieve short corrosion time and corrosion steps simple effect
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[0021] The preparation method of the C55E spring steel spheroidizing annealing corrosion solution in this embodiment includes the following steps: (a) preparing a saturated picric acid aqueous solution, adding picric acid to deionized water and stirring until precipitation occurs; (b) filtering picric acid (c) Add 90-100ml of absolute ethanol; (d) Add concentrated nitric acid and the prepared saturated aqueous solution of picric acid. Through the technical proposal, the C55E spring steel spheroidizing annealing corrosion solution can be conveniently prepared.
[0022] The method for using the spheroidizing annealing corrosion solution for C55E spring steel in this embodiment includes the following steps: (S1) Apply the corrosion solution to the spring steel for a holding time of 2s to 4s; (S2) Wash the surface of the sample with water, and then Rub alcohol and blow dry. Through the above method of use, the spheroidizing annealing solution of the C55E spring steel can clearly ...
Embodiment 1
[0024] The corrosion solution includes: 3.5ml picric acid saturated aqueous solution, 4.5ml concentrated nitric acid, 90ml absolute ethanol.
[0025] Corrosion time: 2s.
[0026] Corrosion effect: the grain boundaries show complete and clear (such as figure 1 shown).
Embodiment 2
[0028] The corrosion solution includes: 3ml picric acid saturated aqueous solution, 7ml concentrated nitric acid, 100ml absolute ethanol.
[0029] Corrosion time: 3s.
[0030] Corrosion effect: The grain boundaries are displayed intact and clear.
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