Environmentally friendly grease and preparation method thereof
A lubricating grease and environmental protection technology, applied in the field of environmentally friendly lubricating grease and its preparation, can solve the problems of not being able to maintain the lubrication effect for a long time, equipment downtime, manpower waste, etc., and achieve good anti-friction and anti-rust effects, good environmental performance, high Effect of Kinematic Viscosity
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Embodiment 1
[0028] Heat 1500g of beeswax to 100°C, heat filter to remove impurities, add 100g of sodium borate into a stirrer, stir and react at 100°C for 3.5 hours, and it is an environmentally friendly grease precursor.
[0029] Weigh 300g of environmentally friendly grease precursor and 700g of polyricinoleic acid ester and stir at 100°C for 40 minutes to obtain an environmentally friendly grease.
[0030] The preparation method of above-mentioned polyricinoleic acid ester is:
[0031] Step 1: 1000g ricinoleic acid and catalyst (5g sodium perborate) are dropped into the polymerization kettle respectively;
[0032] Step 2: Filling with nitrogen to replace the air in the polymerization kettle;
[0033] Step 3: heat up to 200°C while stirring, and react for 4.5 hours;
[0034] Step 4: removing water under reduced pressure to obtain the product.
[0035] The environment-friendly grease prepared above was subjected to roller stability test according to SH / T0122:
[0036] projec...
Embodiment 2
[0038] Heat 2000g of beeswax to 110°C, heat filter to remove impurities, add 100g of potassium tetraborate into a stirrer, stir and react at 100°C for 3 hours, and it is an environmentally friendly grease precursor.
[0039] Weigh 200g of environmentally friendly grease precursor and 800g of polyricinoleic acid ester and stir at 110°C for 30 minutes to obtain an environmentally friendly grease.
[0040] The preparation method of above-mentioned polyricinoleic acid ester is:
[0041] Step 1: 1000g ricinoleic acid and catalyzer (15g cationic catalytic resin) are dropped into polymerization kettle respectively;
[0042] Step 2: Filling with nitrogen to replace the air in the polymerization kettle;
[0043] Step 3: heat up to 180°C while stirring, and react for 5 hours;
[0044] Step 4: removing water under reduced pressure, removing the cationic catalytic resin, and obtaining the product.
Embodiment 3
[0046] Heat 1000g of beeswax to 90°C, heat filter to remove impurities, add 100g of potassium metaborate into a stirrer, stir and react at 90°C for 5 hours, and it is an environmentally friendly grease precursor.
[0047] Weigh 500g of environmental grease precursor and 500g of polyricinoleic acid ester and stir at 90°C for 60 minutes to obtain an environmentally friendly grease.
[0048] The preparation method of above-mentioned polyricinoleic acid ester is:
[0049] Step 1: 1000g ricinoleic acid and catalyst (4g potassium perborate) are dropped into the polymerization kettle respectively;
[0050] Step 2: Filling with nitrogen to replace the air in the polymerization kettle;
[0051] Step 3: heat up to 220°C while stirring, and react for 4 hours;
[0052] Step 4: removing water under reduced pressure to obtain the product.
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