Preparation method of regenerated cellulose/inorganic nano-material composite film
A technology of inorganic nanomaterials and regenerated cellulose, which is applied in the field of preparation of regenerated cellulose/inorganic nanomaterial composite membranes, can solve the problems of poor performance, poor softness, high pollution, etc., and achieve good slipperiness and tensile strength Good, good softness effect
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Embodiment 1
[0026] A preparation method of regenerated cellulose / lithium alginate nanomaterial composite film, comprising the following steps:
[0027] (1) Preparation of an aqueous suspension of leucite: disperse leucite nanomaterials in water, disperse at a high speed for 30 minutes, and obtain a uniform suspension, and the mass percentage of leucite nanomaterials is 2%;
[0028] (2) Preparation of 1-allyl-3-methylimidazolium chloride (AmimCl) ionic liquid suspension of lithium diatomaceous earth: the water suspension of prepared lithium diatomaceous earth is added to a mass fraction of 60.0% In the ionic liquid aqueous solution, the amount of lethonite added accounted for 0.05% of the mass percentage of pure AmimCl, stirred and mixed for 30 minutes, and then dewatered and concentrated until the water content of the solution was 95%;
[0029] (3) Preparation of cellulose / lithium-ionic liquid solution: mix the cellulose raw material with the AmimCl ionic liquid suspension of the concentr...
Embodiment 2
[0041] A preparation method of regenerated cellulose / silicon dioxide nanomaterial composite film, comprising the following steps:
[0042] (1) Preparation of an aqueous suspension of silicon dioxide: disperse the silicon dioxide nanomaterial in water, disperse at high speed for 15 minutes, and obtain a uniform suspension, the mass percentage of the silicon dioxide nanomaterial is 0.5%;
[0043] (2) Preparation of 1-butyl-3-methylimidazole acetate (BmimAc) ionic liquid suspension of silicon dioxide: the aqueous suspension of silicon dioxide prepared is added to a mass fraction of 40.0% In the ionic liquid aqueous solution, the amount of silicon dioxide added accounts for 0.15% of the mass percentage of pure BmimAc, stirred and mixed for 50min, and then dewatered and concentrated until the water content of the solution is 98%;
[0044] (3) Preparation of cellulose / silicon dioxide-ionic liquid solution: mix the cellulose raw material with the concentrated ionic liquid suspension ...
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