Preparation method of pure natural radix polygoni multiflora liquid shampoo
A technology of Polygonum multiflorum and shampoo, applied in the field of shampoo derived from plants and its preparation, can solve the problems of unfavorable environmental protection waste water, waste residue, hair side effects, etc., and achieve the effect of simple and convenient source, less solvent consumption, and rich foam
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Embodiment 1
[0027] Step (1): Crush 150g of freshly squeezed Camellia oleifera cake, pass through a 40-mesh sieve, put the wet sample in boiling water evenly into a glass chromatography column with a diameter of 5cm, soak in the column for 60 minutes, and elute with boiling water. The liquid flow rate was 600 mL / h, and 900 mL of the eluent was collected, concentrated to 600 mL under reduced pressure;
[0028] Step (2): Sun-dry or dry fresh acacia, weigh 200g, crush, pass through a 40-mesh sieve, put the wet sample in boiling water evenly into a glass chromatography column with a diameter of 6 cm, soak in the column for 90 min, boil water For elution, the eluent flow rate is 800 mL / h, and the eluent is collected at 1200 mL;
[0029] Step (3): Slice the raw Polygonum multiflorum, dry it, take 150 g and crush it, pass it through a 40-mesh sieve, put the wet sample with 30% ethanol (v / v) evenly into a glass chromatography column with a diameter of 5 cm, and put it in the column. Soak for 60 m...
Embodiment 2
[0034] Step (1): Crush 200g of freshly squeezed Camellia oleifera cake, pass through a 60-mesh sieve, put the wet sample in boiling water into a glass chromatography column with a diameter of 6cm, soak in the column for 90 minutes, and elute with boiling water. The liquid flow rate was 800 mL / h, and the eluate was collected at 1200 mL, concentrated under reduced pressure to 800 mL;
[0035] Step (2): Sun-dry or dry fresh acacia, weigh 150 g, crush, pass through a 60-mesh sieve, put the wet sample in boiling water evenly into a glass chromatography column with a diameter of 5 cm, soak in the column for 80 min, Elute with boiling water, the eluent flow rate is 800 mL / h, collect 1200 mL of eluent, and concentrate under reduced pressure to 800 mL;
[0036] Step (3): Slice the raw Polygonum multiflorum, dry it, take 200g and crush it, pass it through a 50-mesh sieve, put the wet sample with 50% ethanol (v / v) evenly into a glass chromatography column with a diameter of 5 cm, and soa...
Embodiment 3
[0041] Step (1): crush 180 g of freshly squeezed Camellia oleifera cake, pass through a 50-mesh sieve, put the wet sample in boiling water into a glass chromatography column with a diameter of 5.5 cm, soak in the column for 70 min, and elute with boiling water. The flow rate of eluent is 800 mL / h, and 1000 mL of eluent is collected;
[0042] Step (2): Sun-dry or dry the fresh saponins, weigh 180g, crush, pass through a 50-mesh sieve, put the wet sample in boiling water evenly into a glass chromatography column with a diameter of 5.5 cm, soak the column for 80 min, boil water For elution, the flow rate of the eluent is 700 mL / h, and 1000 mL of the eluent is collected and concentrated to 700 mL under reduced pressure;
[0043] Step (3): Slice the raw Radix Polygoni Multiflori, dry it, take 180 g and crush it, pass it through a 50-mesh sieve, put the wet sample with 40% ethanol (v / v) evenly into a glass chromatography column with a diameter of 5.5 cm, and put it in the column. S...
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