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Agilawood essential oil vacuum fractionation method

The technology of agarwood essential oil and vacuum fractionation, which is applied in the field of essential oil fractionation, can solve the problems of poor quality, low fractionation efficiency and high cost of agarwood essential oil fractionation, and achieves the effects of convenient control, guaranteed collection purity, and accelerated rapid distillation.

Inactive Publication Date: 2018-03-06
广东贡品沉香产业投资有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In view of this, the present invention provides a method of vacuum fractionation of agarwood essential oil with lower cost and higher fractionation efficiency to solve the problems of poor fractionation quality, low fractionation efficiency and high cost of agarwood essential oil in the prior art

Method used

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  • Agilawood essential oil vacuum fractionation method
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  • Agilawood essential oil vacuum fractionation method

Examples

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Effect test

Embodiment 1

[0090] A kind of agarwood essential oil vacuum fractionation method, adopts Figure 1-4 device to run, including the following steps:

[0091] (1) Preliminary preparation:

[0092] crushing agarwood wood into agarwood powder with a particle size of 40-60 meshes, and then extracting the agarwood by a supercritical fluid extraction method to obtain an agarwood essential oil extract;

[0093] Place the agarwood essential oil extract in the raw material tank 1 and preheat it to 70°C; preheat the distiller 12 to 130°C, preheat the scraping film 16 to 130°C, and precool the condenser tube 20 to 26°C; then The vacuum degree in the distiller 12 reaches 3.0Pa by the vacuum pump 4; The vacuum degree in the distiller 12 reaches 1.0Pa by the diffusion pump 3;

[0094] (2) Fractionation process:

[0095] The preheated agarwood essential oil extract flows out from the raw material tank 1, and is added into the still 1 along the tube wall of the still 2 at a speed of 80mL / s; The membrane...

Embodiment 2

[0110] A kind of agarwood essential oil vacuum fractionation method, adopts Figure 1-4 device to run, including the following steps:

[0111] (1) Preliminary preparation:

[0112] Crushing the agarwood wood into agarwood powder with a particle size of 60 meshes, and then extracting it with a supercritical fluid extraction method to obtain an agarwood essential oil extract; placing the agarwood essential oil extract in the raw material tank 1, and preheating to 60°C;

[0113] The distiller 12 is preheated to 122°C, the wiper film 16 is preheated to 122°C, and the condenser tube 20 is precooled to 30°C; The vacuum degree in distiller 12 reaches 1.2Pa;

[0114] (2) Fractionation process:

[0115] The preheated agarwood essential oil extract flows out from the raw material tank 1, and is added into the still 1 along the tube wall of the still 2 at a speed of 90mL / s; the scraper control device 14 drives the scraper at a speed of 400r / min The diaphragm 16 rotates, and the scrap...

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Abstract

The invention provides an agilawood essential oil vacuum fractionation method. The agilawood essential oil vacuum fractionation method comprises the following steps: preheating a distiller to 110-140DEG C, pumping the pressure of the interior of the distiller to be no higher than 3.8Pa; adding a preheated agilawood essential oil extract in the distiller along the pipe wall of the distiller; controlling a film scraping device with the lower end extending into the distiller to drive a film scraping sheet connected to the lower end of the film scraping device to rotate, scraping off the agilawood essential oil extract from the pipe wall of the distiller by the film scraping device, dispersing the agilawood essential oil extract on the film scraping sheet preheated to 110-140 DEG C, evaporating an essential oil fractionation component from the agilawood essential oil extract, draining to a condenser pipe from the distiller, coagulating into a liquid in the pre-cooled condenser pipe, collecting the liquid, enabling a residue component fractionated from the agilawood essential oil extract to fall off from the film scraping sheet, and collecting the residue component in a residue collecting bottle. The fractionation quality is good, the fractionation efficiency of the essential oil is high, and the method has a higher practical value.

Description

technical field [0001] The invention relates to the technical field of essential oil fractionation, in particular to a vacuum fractionation method for agarwood essential oil. Background technique [0002] Agarwood is the resinous wood of Aquilaria sinensis (Lour.) Gilg, a plant of the family Thymelaeaceae. Distributed in Guangdong, Hainan, Guangxi, Fujian and other places. Agarwood essential oil is distilled and extracted from precious agarwood, which is the essence of agarwood. Agarwood essential oil has multiple effects on the human body, such as: improving the aura, relieving stress, sleeping and anti-depression, regulating the body and mind, and promoting body metabolism. A few drops of agarwood essential oil can be added to the hot water for soaking feet to achieve the purpose of promoting blood circulation and meridians, and can also achieve the effect of removing beriberi and foot odor. Due to the non-renewability of natural agarwood, the refined agarwood oil is ev...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02
CPCC11B9/027
Inventor 李亚泳覃全业
Owner 广东贡品沉香产业投资有限公司
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