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Process for extracting pectin by using sisal hemp residue

A technology of sisal residue and pectin, which is applied in the field of pectin extraction, can solve the problems of no large-scale production, small safety factor, and high production cost, so as to prevent volatilization and unnecessary loss, improve product performance, and increase profitability effect of space

Inactive Publication Date: 2018-01-26
杭州舒诚生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] 2. Acidic extraction has high requirements on system equipment, resulting in an increase in equipment investment
[0007] 3. Low product yield, high energy consumption and high production cost
Although the economic benefits of pectin manufacturers with the old technology are relatively good, due to the defects of the old technology, there is no large-scale production manufacturer (the largest actual monthly production is no more than 40 tons)
[0009] 4. The initial concentration is low, the amount of liquid that needs to be concentrated and evaporated is huge, the energy consumption is high, and the production cost is high
[0010] The initial concentration of the pectin extract in the existing old process is 0.4% to 0.5% (1.5% in the patented process) and needs to be increased by 30 times (10 times in the patented process) to concentrate to a crystallizable concentration of 15%, so the energy consumption is huge. Accounted for about 40% of the entire production cost
[0011] 5. The product quality is relatively poor
[0013] 6. Large investment in safety facilities during production
One is that the loss of organic solvent is large, and the other is that after the organic solvent is used, it is flammable and explosive, the safety factor is small, and the investment in safety protection is also large.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] The present invention provides a kind of process utilizing sisal residue to extract pectin, comprising steps:

[0043] S1. Raw material pretreatment

[0044] Squeeze the fresh sisal slag until dry and pulverize it, and finally dry the crushed sisal slag;

[0045] S2, cooking to kill enzymes

[0046] Accurately measure 1000 parts of deionized water into the stainless steel reactor, stir and steam heat to 65°C, then add 50 parts of sisal dry residue, continue to heat up to 85°C, keep warm in this temperature range for 80 minutes to kill enzymes, and then press again until dry, the secondary wet slag of sisal is obtained;

[0047] S3, near-neutral extraction of inorganic salts

[0048] Slowly add inorganic salt additives into the glass-lined reaction kettle and add 1000 parts of deionized water, and then steam-heat to 65°C, slowly and continuously add 80 parts of the above-mentioned secondary wet residue of sisal, and continue to heat up to 83°C after the heating is com...

Embodiment 2

[0068] The present invention provides a kind of process utilizing sisal residue to extract pectin, comprising steps:

[0069] S1. Raw material pretreatment

[0070] Squeeze the fresh sisal slag until dry and pulverize it, and finally dry the crushed sisal slag;

[0071] S2, cooking to kill enzymes

[0072] Accurately measure 1000 parts of deionized water and add it into the stainless steel reaction kettle for stirring and steam heating to 75°C, then add 50 parts of sisal dry residue, continue to heat up to 88°C, keep warm in this temperature range for 80-100 minutes to kill the enzyme, and then Squeeze again until dry to obtain the secondary wet residue of sisal;

[0073] S3, near-neutral extraction of inorganic salts

[0074] Slowly add inorganic salt additives into the glass-lined reactor and add 1000 parts of deionized water, and then steam-heat to 75°C, slowly and continuously add 80 parts of the above-mentioned secondary wet residue of sisal, and continue to heat up to...

Embodiment 3

[0090] The present invention provides a kind of process utilizing sisal residue to extract pectin, comprising steps:

[0091] S1. Raw material pretreatment

[0092] Squeeze the fresh sisal slag until dry and pulverize it, and finally dry the crushed sisal slag;

[0093] S2, cooking to kill enzymes

[0094] Accurately measure 1000 parts of deionized water into the stainless steel reactor, stir and steam heat to 80°C, then add 50 parts of sisal dry residue, continue to heat up to 90°C, keep warm in this temperature range for 100 minutes, and then press again until dry, the secondary wet slag of sisal is obtained;

[0095] S3, near-neutral extraction of inorganic salts

[0096] Slowly add inorganic salt additives into the glass-lined reaction kettle and add 1000 parts of deionized water, and then steam-heat to 80°C, slowly and continuously add 80 parts of the above-mentioned secondary wet residue of sisal, and continue to heat up to 88°C after the heating is completed. Heat p...

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PUM

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Abstract

The invention discloses a process for extracting pectin by using sisal hemp residue. The process comprises: S1, raw material pretreatment; S2, enzyme inactivation through cooking; S3, near neutral extraction with an inorganic salt; S4, decolorization and impurity removal; S5, pressure reducing concentration; S6, crystallization; S7, three treatment combination; and S8, drying screening and pectinfinished product obtaining. According to the present invention, the solid technical basis is provided for the large-scale production of pectin and the ensuring of the normal pectin product supply through the rich raw material resources; the pectin is extracted by using the neutral inorganic salt as the auxiliary agent, such that the investment on the production equipment can be save about 30%; theproduced pectin is the natural low-fat pectin, such that the performance of the product is further improved, and the process has advantages of simpleness, effectiveness, safety, low cost and good benefits; and with the process, the volatilization of organic solvents and the unnecessary loss are effectively prevented, the pectin production safety achieves the relatively improved assurance, the loss of organic solvents is substantially reduced, the production cost is reduced, and the profit of pectin enterprises can be increased.

Description

technical field [0001] The invention relates to the application field of pectin extraction, in particular to a process for extracting pectin by using sisal residue. Background technique [0002] At present, the domestic pectin extraction process is usually, citrus peel (apple peel)→pretreatment→acid extraction→decompression concentration→decolorization→filtrationcrystallization→washing→centrifugation→secondary washing→secondary centrifugationdrying→pectin finished product . However, with the continuous development of society and the continuous change of industry, the above-mentioned pectin extraction process has the following problems: [0003] 1. The raw materials used are relatively scarce, and the product supply cannot be stable and timely. [0004] The citrus peel that existing old technology adopts is to utilize the leftover waste of citrus canned food manufacturer, and the used raw material of producing apple pectin is also the discarded material after the apple sq...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08B37/06
Inventor 舒大伟
Owner 杭州舒诚生物科技有限公司
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