Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Food-grade fluorescent nano-microemulsion and preparation method thereof

A fluorescent nano, food-grade technology, applied in the field of preparation of fluorescent nano-microemulsions, can solve the problems of undiscovered optical properties of fluorescent micro-emulsions, etc., and achieve simple and easy-to-obtain raw materials, good biocompatibility, and low preparation costs Effect

Inactive Publication Date: 2017-11-24
TIANJIN UNIV
View PDF3 Cites 4 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] At present, the preparation and research of microemulsions are mainly focused on their physical and chemical properties and related applications, and no literature on fluorescent microemulsions and their optical properties has been found.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] A preparation method for food-grade fluorescent nano-microemulsion, comprising the steps of:

[0029] (1) Mix 90mg of isoamyl acetate and 30mg of absolute ethanol to obtain a mixed oil phase, then add 1.5 times the quality of the mixed oil phase, that is, 180mg CrEL, mix it in a small beaker, add the rotor, adjust the rotating speed to 150rpm, Stir for 10 minutes at 4°C;

[0030] (2) At a stirring speed of 150rpm, add water dropwise, the total mass of the added water is 1.5 times the total mass of the liquid obtained in step (1), to obtain a uniform, transparent food-grade fluorescent nano-microemulsion.

[0031] The particle diameter of the obtained microemulsion is 26.34nm, the PDI (polydispersity Index) is 0.309, and the fluorescence intensity is near 8000.

Embodiment 2

[0033] A preparation method for food-grade fluorescent nano-microemulsion, comprising the steps of:

[0034] (1) Mix 90mg of isoamyl acetate and 60mg of absolute ethanol to obtain a mixed oil phase, then add 3 times the mass of the mixed oil phase, that is, 450mg CrEL, and mix it in a small beaker, add the rotor, adjust the rotating speed to 200rpm, Stir for 20min at 25°C;

[0035] (2) At a stirring speed of 200rpm, add water dropwise, and the total mass of the added water is 2.33 times the total mass of the liquid obtained in step (1); obtain a uniform, transparent food-grade fluorescent nano-microemulsion.

[0036] The particle diameter of the obtained microemulsion is 25.62nm, the PDI (polydispersity Index) is 0.323, and the fluorescence intensity is near 8200.

Embodiment 3

[0038] A preparation method for food-grade fluorescent nano-microemulsion, comprising the steps of:

[0039] (1) Mix 40mg of isoamyl acetate and 40mg of absolute ethanol to obtain a mixed oil phase, then add 6 times the mass of the mixed oil phase, that is, 480mg CrEL, mix in a small beaker, add the rotor, adjust the rotating speed to 250rpm, Stir for 30min at 50°C;

[0040] (2) At a stirring speed of 250rpm, add water dropwise, and the total mass of the added water is 4 times the total mass of the liquid obtained in step (1); obtain a uniform and transparent food-grade fluorescent nano-microemulsion.

[0041] The particle diameter of the obtained microemulsion is 23.24nm, the PDI (polydispersity Index) is 0.378, and the fluorescence intensity is near 7500. Example 4

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
Particle sizeaaaaaaaaaa
Particle sizeaaaaaaaaaa
Particle sizeaaaaaaaaaa
Login to View More

Abstract

The invention discloses a food-grade fluorescent nano-microemulsion and a preparation method thereof. The preparation method comprises the following steps: (1) mixing isoamyl acetate with ethanol, so as to obtain a mixed oil phase, adding polyoxyethylated castor oil, and stirring; and (2) dropwise adding water while stirring, so as to obtain uniform and transparent food-grade fluorescent nano-microemulsion. The oil-in-water food-grade fluorescent nano-microemulsion prepared by virtue of the preparation method has fluorescence characteristics, belongs to the field of food-grade nano-fluorescent materials, is toxic free and biodegradable and has good biocompatibility. The food-grade fluorescent nano-microemulsion does not need to be labeled when being used as a fluorescent nano-material, and no bracket is needed. The adopted raw materials are simple and easily available, isoamyl acetate is an aromatic additive for foods, the preparation cost of the product is low, and meanwhile, the food-grade fluorescent nano-microemulsion further has special fragrance. The high-temperature and high-pressure treatment is not required in the preparation method, and the preparation method is simple, feasible and high in process efficiency and meets the concepts of energy conservation and environment protection.

Description

technical field [0001] The invention relates to a method for preparing fluorescent nanometer microemulsion, which belongs to the field of production, preparation and application of microemulsion. Background technique [0002] For a long time, the research on functional factors in food and medicine has not been interrupted, and most of them focus on evaluating their physiological activities through cell and animal experiments, and the research on their mechanism of action is very difficult. The emergence and application of food-grade fluorescent probes can more intuitively detect some changes of functional factors in vivo and in vitro, so as to realize real-time monitoring of functional factors. [0003] Based on the extensive research on fluorescent materials, the research on fluorescent nanomaterials has set off a new wave. Phosphors are based on sensors that convert chemical, physical, biological, and other difficult-to-detect information into optical information for dete...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C09K11/06C08J3/03C08L71/02
CPCC09K11/06C08J3/03C08J2371/02
Inventor 王占忠侯梦娜李卿陆超党乐平
Owner TIANJIN UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products