Benzothiostrobin-containing controlled-release composition and preparation method thereof
A technology of Benthoxystrobin and the composition is applied in the controlled-release composition containing Benthoxystrobin and the field of preparation thereof, which can solve problems such as unfavorable environmental protection and achieve the effect of reducing toxicity
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Embodiment 1
[0078] Example 1: Preparation of nano-formulation bactericide
[0079] (1) 100mg of nano-silica particles (average particle size of 50nm) are contacted with 100mL of water to form a mixture A, and 100mg of methiophene and 2mL containing emulsifier (Tween 80) and stabilizer (polyethylene Glycol diglycidyl ether) methanol solution (in the methanol solution, the methanol content is 88.98% by weight, the content of Tween 80 is 8.47% by weight, and the content of polyethylene glycol diglycidyl ether is 2.55% by weight) contact To form solution A;
[0080] (2) contacting the solution A of step (1) with the mixture A of step (1) under stirring to obtain solution B;
[0081] (3) Contacting 300 mg of sodium alginate with the solution B of step (2) under stirring to obtain suspension A;
[0082] (4) Dissolve 300 mg of magnesium chloride in 10 mL of water to obtain solution C, and contact this solution C with the suspension A of step (4) to obtain suspension B;
[0083] (5) Remove the solvent in...
Embodiment 2
[0091] Example 2: Preparation of nano-formulation bactericide
[0092] (1) 100mg of nano-silica particles (average particle size of 50nm) are contacted with 100mL of water to form a mixture A, and 500mg of methiophene and 8mL containing emulsifier (Tween 80) and stabilizer (polyethylene Glycol diglycidyl ether) methanol solution (in the methanol solution, the methanol content is 87.69% by weight, the content of Tween 80 is 6.39% by weight, and the content of polyethylene glycol diglycidyl ether is 5.92% by weight) contact To form solution A;
[0093] (2) contacting the solution A of step (1) with the mixture A of step (1) under stirring to obtain solution B;
[0094] (3) Contacting 500 mg of sodium alginate with the solution B of step (2) under stirring to obtain suspension A;
[0095] (4) Dissolve 320 mg of calcium chloride in 10 mL of water to obtain solution C, and contact this solution C with the suspension A of step (4) to obtain suspension B;
[0096] (5) Remove the solvent in t...
Embodiment 3
[0098] Example 3: Preparation of nano-formulation bactericide
[0099] (1) Contact 150mg of nano-silicon particles (with an average particle size of 60nm) with 100mL of water to form mixture A, and 720mg of Benthiastrobin with 10mL containing emulsifier (Tween 80) and stabilizer (polyethylene glycol Diglycidyl ether) methanol solution (in the methanol solution, the methanol content is 89.31 wt%, the content of Tween 80 is 6.92 wt%, and the content of polyethylene glycol diglycidyl ether is 3.77 wt%) to form Solution A;
[0100] (2) contacting the solution A of step (1) with the mixture A of step (1) under stirring to obtain solution B;
[0101] (3) Contact 600 mg of sodium alginate with the solution B of step (2) under stirring to obtain suspension A;
[0102] (4) Dissolve 380 mg of magnesium chloride in 10 mL of water to obtain solution C, and contact the solution C with the suspension A of step (4) to obtain suspension B;
[0103] (5) Remove the solvent in the suspension B by spray ...
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