A method for preparing gold nanoparticles by utilizing Panax notoginseng extract
A nanoparticle and extraction liquid technology, applied in the field of materials science, can solve the problems of complex process of gold nanoparticles and easy environmental pollution, and achieve the effect of remarkable technological progress, environmental friendliness and low price.
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Embodiment 1
[0030] (1) Wash the glass container used with deionized water;
[0031] (2) Put 10 mL of Panax notoginseng extract and 15 mL of deionized water into the flask, then add 200 μL of sodium hydroxide solution and heat to boiling for 5 minutes;
[0032] (3) Add 100 μL of 0.1 mol / L chloroauric acid solution to the flask, test the pH value to 5.75, and react under boiling conditions for 2 minutes, 5 minutes, 10 minutes, 15 minutes, and 20 minutes and then take samples. Sample photos such as figure 1 .
[0033] (4) The samples obtained after different reaction times were centrifuged at 8000 rpm for 10 minutes, and the obtained precipitate was dried at 40-50° C. for 10 minutes to obtain gold nanoparticles.
[0034] figure 2 In order to use the UV-2600 UV spectrophotometer of Shimadzu Corporation of Japan to centrifuge the samples obtained from the above reaction for 2 minutes, 5 minutes, 10 minutes, 15 minutes and 20 minutes to measure their UV-Vis absorption spectrum (UV-Vis.) Fig...
Embodiment 2
[0038] (1) Wash the glass container used with deionized water;
[0039] (2) Put 10 mL of Panax notoginseng extract and 15 mL of deionized water into the flask, then add 100 μL of sodium hydroxide solution and heat to boiling, and let it boil for 10 minutes;
[0040] (3) Add 100 μL of chloroauric acid solution to the flask, test the pH value of 5.25, and react under boiling conditions for 2 minutes, 5 minutes, 10 minutes, 15 minutes, and 20 minutes and then take samples. Sample photos such as Figure 5 .
[0041] (4) The samples obtained after different reaction times were centrifuged at 8000 rpm for 10 minutes, and the obtained precipitate was dried at 40-50° C. for 10 minutes to obtain gold nanoparticles.
[0042] Image 6 In order to use the UV-2600 UV spectrophotometer of Shimadzu Corporation of Japan to centrifuge the samples obtained from the above reaction for 2 minutes, 5 minutes, 10 minutes, 15 minutes and 20 minutes to measure their UV-Vis absorption spectrum (UV-V...
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