High-mid-infrared barrier and high-light transmittance PVB film and making method thereof
A technology with high light transmittance and high barrier, which is applied in the field of mid-infrared high barrier and high transmittance PVB film and its preparation, can solve the problems of high cost, low light transmittance and large haze of heat-insulating PVB film, and achieve Improved layering, superior mid-IR blocking and reflective capabilities, and production process optimization
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Embodiment 1
[0039] (1) Preparation of DST nano-dispersion liquid: After mixing 8.5kg of organic solvent triethylene glycol diisocaprylate, 0.8kg of nano-ITO powder and 0.2kg of nano-GATO powder, add 0.5kg of dispersant during slow grinding Silane coupling agent 6598, continue to grind on a ball mill for 24 hours to obtain a nano-DST dispersion.
[0040] (2) 100kgPVB resin powder, 0.5kg antioxidant mixture (from 266.8g tetrakis [β-(3,5-di-tert-butyl-4-hydroxyphenyl) propionic acid] pentaerythritol ester and 133.2g three [2, 4-di-tert-butylphenyl]phosphite), 0.1kg UV absorber mixture (composed of 50g 2-(2'-hydroxy-5'-tert-octyl)-benzotriazole and 50g2-(2'-hydroxy- 5'-methyl)-benzotriazole), added to the powder mixer, and stirred at a high speed of 1000RPM for 20 minutes. Control the temperature of the equipment so that the temperature of the material during the stirring process is between 40°C and 50°C. Finally, 38 kg of plasticizer triethylene glycol diisocaprylate and 1 kg of nano-DST d...
Embodiment 2
[0042] (1) Preparation of DST nano-dispersion liquid: After mixing 8.5kg of organic solvent triethylene glycol diisocaprylate, 0.6kg of nano-ITO powder and 0.4kg of nano-GATO powder, add 0.5kg of dispersant during slow grinding Silane coupling agent 6598, continue to grind on a ball mill for 24 hours to obtain a nano-DST dispersion.
[0043] (2) 100kgPVB resin powder, 0.5kg antioxidant mixture (from 266.8g tetrakis [β-(3,5-di-tert-butyl-4-hydroxyphenyl) propionic acid] pentaerythritol ester and 133.2g three [2, 4-di-tert-butylphenyl]phosphite), 0.1kg UV absorber mixture (composed of 50g 2-(2'-hydroxy-5'-tert-octyl)-benzotriazole and 50g2-(2'-hydroxy- 5'-methyl)-benzotriazole), added to the powder mixer, and stirred at a high speed of 1000RPM for 20 minutes. Control the temperature of the equipment so that the temperature of the material during the stirring process is between 40°C and 50°C. Finally, 38 kg of plasticizer triethylene glycol diisocaprylate and 1 kg of nano-DST d...
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