Determination method of fluorine, chlorine, sulfur and nitrogen in imported petroleum coke
A determination method and technology of petroleum coke, applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve problems such as lack of detection methods, and achieve the effect of simple method
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[0051] Instruments and reagents
[0052] Instruments: DIONEX AQUION ion chromatograph (ThermoFisher, USA) and DIONEX AS-DV autosampler (ThermoFisher, USA), equipped with DIONEX RFC-30 eluent automatic generator and Chromeleon chromatography workstation. Tubular high-temperature furnace (Shanghai Institute of Optics and Fine Mechanics); platinum-rhodium-platinum thermocouple (Omega Corporation, USA); pressure reducing valve (Danyang Leicester Fluid Products Co., Ltd.); flowmeter (Changzhou Tiansheng Thermal Instrument Co., Ltd. company); 0.22 μm microporous cellulose membrane and membrane filtration (Agilent, USA); ultrapure water machine (Milli-Q).
[0053] Reagent: F - , Cl - , SO 4 2- , NO 3 - 、PO 4 3- Mixed standard solution (100mg / L, 250mg / L, 500mg / L, 500mg / L, 1000mg / L, Germany MERCK company); quartz sand (particle size 0.5mm~1.0mm, Tianjin Kemiou Chemical Reagent Co., Ltd.); Oxygen (purity ≥ 99.999%, Shanghai Chemical Industry Zone Pujiang Special Gas Co., Ltd.);...
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