Degradable fracturing propping agent and preparation method thereof
A fracturing proppant and solvent technology, which is applied in chemical instruments and methods, earthwork drilling, production of fluids, etc., can solve the problems that the research on degradable fracturing proppant has not been reported, and achieves low price, simple preparation process, and low cost. cost effect
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[0030] This embodiment provides a degradable fracturing proppant, which is prepared by the following steps:
[0031] The preparation of modified starch: in the aqueous solution of modifying agent (maleic anhydride 0.15g, sodium periodate 0.12g, phosphorus oxychloride 0.08g), appropriate amount of starch agent (dimethyl dimethylformamide 2.30) to cornstarch 10kg was improved, and the product was dried at 70°C for later use;
[0032] Preparation of copolymer: gelatinize 8kg of the above-mentioned modified starch and 100L of lactic acid at 80°C for 1.5 hours, dehydrate under vacuum (0.085MPa) at 105°C until the system has no bubbles and no water vapor flows out, and then add 0.60g of zinc oxide, caprylic acid 0.45 g of stannous was reacted at 130°C for 5 hours, and at 140°C for 15 hours; the product was dissolved in chloroform (insoluble matter was removed by filtration), precipitated with methanol, centrifuged, the product was dissolved and precipitated repeatedly, and the preci...
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