Polylactic acid fresh-keeping film containing natural antibacterial ingredients and preparation method thereof
A natural antibacterial and polylactic acid technology, which is applied to biocide-containing paints, coatings, antifouling/underwater coatings, etc., can solve the problems of loss of antibacterial materials, white pollution, waste, etc., and achieve coating drying time is small, The processing method is simple, and the effect of solving white pollution
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Embodiment 1
[0030] To prepare the ethyl acetate extract of fig branches, take the naturally dried fig branches, crush them through a 40-mesh sieve, use the Soxhlet extraction method, use ethyl acetate as the extractant and reflux at 60°C for 6 hours, take the ethyl acetate extract, and medium-speed Filter through filter paper, evaporate the ethyl acetate to dryness under vacuum at 35°C, and the remaining viscous substance is the ethyl acetate extract of fig branches.
[0031] A kind of polylactic acid protective film containing natural antibacterial composition prepared by the present invention is divided into three steps:
[0032] The first step is to prepare the modified polylactic acid film
[0033] 99% by weight of polylactic acid particles (REVODE110) and 1% by weight of nano-copper (CW-Cu-001) were mixed uniformly by a high-speed mixer, and blown by a film blowing machine to form a modified polylactic acid film.
[0034] The second step is to prepare antibacterial coating
[0035]...
Embodiment 2
[0045] A kind of polylactic acid protective film containing natural antibacterial composition prepared by the present invention is divided into three steps:
[0046] The first step is to prepare the modified polylactic acid film
[0047] 99.5% by weight of polylactic acid particles (REVODE110) and 0.5% by weight of nano-copper (CW-Cu-001) were mixed uniformly by a high-speed mixer, and blown by a blown film machine to form a modified polylactic acid film.
[0048] The second step is to prepare antibacterial coating
[0049] The weight percentages of each component are as follows:
[0050] Fig branch ethyl acetate extract 2%;
[0051] Acrylic acid-hydroxypropyl acrylate copolymer 95%;
[0052] Hydroxypropyl Acrylate 2%;
[0053] Initiator BP1173 1%
[0054] Add the above components into a high-speed mixer at a speed of 600r / min and stir evenly, and seal it for later use.
[0055] The third step, coating
[0056] The sealed antibacterial coating is passed through a roller...
Embodiment 3
[0059] A kind of polylactic acid protective film containing natural antibacterial composition prepared by the present invention is divided into three steps:
[0060] The first step is to prepare the modified polylactic acid film
[0061] 99.8% by weight of polylactic acid particles (REVODE110) and 0.2% by weight of nano-copper (CW-Cu-001) were mixed uniformly by a high-speed mixer, and blown by a blown film machine to form a modified polylactic acid film.
[0062] The second step is to prepare antibacterial coating
[0063] The weight percentages of each component are as follows:
[0064] Fig branch ethyl acetate extract 1.5%;
[0065] Acrylic acid-hydroxypropyl acrylate copolymer 80%;
[0066] Multifunctional acrylate monomer 16.5%;
[0067] Initiator BP1173 2%
[0068] Add the above components into a high-speed mixer at a speed of 600r / min and stir evenly, and seal it for later use.
[0069]The third step, coating
[0070] Pass the sealed antibacterial coating on the ...
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