A method for removing scale and heavy metal ions in water
A heavy metal ion and water removal technology, applied in the field of water treatment, can solve the problems of weak adsorption capacity of graphene/carbon nanotube composite materials, agglomeration of graphene and carbon nanotubes, and low orderly arrangement of carbon nanotubes, etc. The effect of mild conditions, good adsorption capacity and convenient operation
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Embodiment 1
[0034] Step 1 Pretreatment of carbon nanotubes:
[0035] Disperse 1g of original multi-walled carbon nanotubes (prepared by chemical vapor deposition) into a mixed acid solution consisting of 30ml of concentrated sulfuric acid and 10ml of concentrated nitric acid, stir and react at 60°C for 3 hours, wash with distilled water until neutral, and dry in vacuum at 80°C Reserve after 12 hours.
[0036] The preparation of step 2 graphene oxide:
[0037] Take 2g of natural flake graphite with an electronic balance, use a graduated cylinder to measure 46ml of concentrated sulfuric acid and pour it into a 1000ml three-neck bottle, cool to 0~5°C, add the weighed 2g of graphite to 46ml of concentrated sulfuric acid, Use an ice bath to cool to 0~5°C and stir until the graphite is completely dissolved, add 1g of sodium nitrate and 6g of potassium permanganate at a certain speed while stirring vigorously, keep the temperature of the mixture below 10°C and continue stirring for 2.5 hours; r...
Embodiment 2
[0044] Step 1 Pretreatment of carbon nanotubes:
[0045] Disperse 2 g of original multi-walled carbon nanotubes (prepared by chemical vapor deposition) into a mixed acid solution of 60 ml of concentrated sulfuric acid and 20 ml of concentrated nitric acid, stir and react at 60°C for 3 hours, wash with distilled water until neutral, and dry in vacuum at 80°C for 12 Stand by after hours.
[0046] The preparation of step 2 graphene oxide:
[0047] Take 4g of natural flake graphite with an electronic balance, use a measuring cylinder to measure 92ml of concentrated sulfuric acid and pour it into a 1000ml three-neck bottle, cool to 0~5°C, add the weighed 4g of natural graphite into 92ml of concentrated sulfuric acid , use an ice bath to cool to 0~5°C and stir until the graphite is completely dissolved, add 2g of sodium nitrate and 12g of potassium permanganate at a certain speed while stirring vigorously, keep the temperature of the mixture below 10°C and continue stirring for 2.5...
Embodiment 3
[0054] Step 1 Pretreatment of carbon nanotubes:
[0055] Disperse 0.5g of original multi-walled carbon nanotubes (prepared by chemical vapor deposition) into a mixed acid solution of 15ml of concentrated sulfuric acid and 5ml of concentrated nitric acid, stir and react at 60°C for 3 hours, wash with distilled water until neutral, and dry in vacuum at 80°C Reserve after 12 hours.
[0056] The preparation of step 2 graphene oxide:
[0057] Use an electronic balance to take 2g of natural flake graphite, use a graduated cylinder to measure 46ml of concentrated sulfuric acid and pour it into a 1000ml three-neck bottle, cool to 0~5°C, add the weighed 2g of natural graphite to 92ml of concentrated sulfuric acid , use an ice bath to cool to 0~5°C and stir until the graphite is completely dissolved, add 2g of sodium nitrate and 12g of potassium permanganate at a certain speed while stirring vigorously, keep the temperature of the mixture below 10°C and continue stirring for 2.5 hours;...
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