Composite nanofiltration anti-haze antibiotic inhibition mask based on grapheme oxide and preparing method
A technology of graphene and masks, which is applied in the field of composite nanofiltration anti-haze antibacterial and antibacterial masks based on graphene oxide and its preparation, can solve the problems of comfort, aesthetics, long residence time, and inability to filter PM2.5, etc. Achieve the effects of convenient operation of process equipment, favorable industrialization, and low raw material prices
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Embodiment 1
[0042] The invention also discloses a preparation method of a composite nanofiltration anti-haze antibacterial and antibacterial mask based on graphene oxide, comprising the following steps:
[0043] (1) Spread the polypropylene non-woven fabric base material with an area density of 30g / ㎡ on the inner grounded metal plate 16;
[0044] (2) Mix graphene oxide and nano-silicon dioxide in a ratio of 4:3 in a reaction vessel, and stir and react at 10°C for 1 hour under non-neutral conditions to obtain a graphene oxide / silicon dioxide composite;
[0045] (3) Dissolve the high molecular polymer polyacrylonitrile, graphene oxide / silica composite with a mixing ratio of 5:4 in a solvent with a mixing ratio of methanol and ethanol of 3:1, stir until completely dissolved, and obtain a spinning Solution, the mass percentage concentration of spinning solution is 8wt%;
[0046] (4) Add the spinning solution prepared in step (3) into the syringe pump 12, control the ambient humidity to 20%, ...
Embodiment 2
[0052] The invention also discloses a preparation method of a composite nanofiltration anti-haze antibacterial and antibacterial mask based on graphene oxide, comprising the following steps:
[0053] (1) Spread the polypropylene non-woven fabric base material with an area density of 50g / ㎡ on the internally grounded metal plate 16;
[0054] (2) Mix graphene oxide and nano-silicon dioxide in a ratio of 4:3 in a reaction vessel, and stir and react at 40°C for 8 hours under non-neutral conditions to obtain a graphene oxide / silicon dioxide composite;
[0055] (3) Dissolve the high molecular polymer polyvinylidene fluoride and graphene oxide / silica composite in a mixing ratio of 5:4 in a solvent of formic acid and acetic acid in a mixing ratio of 3:1, and stir until completely dissolved to obtain a spinning Solution, the mass percentage concentration of spinning solution is 15wt%;
[0056] (4) Add the spinning solution prepared in step (3) into the syringe pump 12, control the ambi...
Embodiment 3
[0062] The invention also discloses a preparation method of a composite nanofiltration anti-haze antibacterial and antibacterial mask based on graphene oxide, comprising the following steps:
[0063] (1) Lay 75g / ㎡ polypropylene non-woven fabric substrate on the inner grounded metal plate 16;
[0064] (2) Mix graphene oxide and nano-silicon dioxide in a reaction vessel at a ratio of 4:3, and stir and react at 80°C for 15 hours under non-neutral conditions to obtain a graphene oxide / silicon dioxide composite;
[0065] (3) Dissolve high molecular polymer polyurethane and graphene oxide / silica composite in a mixing ratio of 5:4 in a solvent of formic acid and acetic acid in a mixing ratio of 3:1, stir until completely dissolved to obtain a spinning solution, and spin The mass percentage concentration of silk solution is 20wt%;
[0066] (4) Add the spinning solution prepared in step (3) into the syringe pump 12, control the ambient humidity to 60%, and the ambient temperature to 5...
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Abstract
Description
Claims
Application Information
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