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Preparation method of sterilization medicament and sterilization medicament

A technology of medicament and emulsifier, applied in the field of preparation of bactericidal medicaments, can solve the problems such as loss of control effect of chemical medicaments, rampant pests, increase in application rate, etc. Effect

Inactive Publication Date: 2017-05-03
李海燕
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Chemical agents play an important role in the control of crop diseases and insect pests. However, due to the long-term use of chemical agents, the frequency of resistance to diseases and insect pests in most areas exceeds 50%, and the resistance level is as high as more than 10,000 times. The single use of chemical agents has completely lost the control effect
Moreover, as the resistant strains continue to increase, the number of spraying increases year by year, and the amount of spraying also doubles, which brings great pressure to the control and the surrounding environment.
Its disadvantages are also becoming more and more prominent, such as drug residues, environmental pollution and harmful organisms are rampant again, etc.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] Formula: 0.05g iodine, 3g licorice, 5g skullcap, 0.2g dry alum, 3g honeysuckle, 2g emulsifier, 0.1g phosphoric acid.

[0016] Grind licorice, scutellaria baicalensis, dried alum, and honeysuckle, pass through a 20-40 mesh sieve, add 6-7 times of 30%-70% ethanol to the crushed matter to submerge them all, soak for 24-72 hours, and then infiltrate in a percolator , filter out larger particles, then heat the filtrate to evaporate residual ethanol, and concentrate to a solid-to-liquid ratio of 1:1, then centrifuge or use resin adsorption to filter out fine particles and other impurities, and the resulting filtrate is ready for use.

[0017] Mix iodine with an emulsifier, emulsify and complex into a paste, and set aside.

[0018] Mix the above-mentioned filtrate and paste, stir evenly, then add water to dilute, after stirring evenly, add medical phosphoric acid to adjust the pH to 1.3-2.8, and finally fill and seal to obtain the product.

Embodiment 2

[0020] Formula: 2g iodine, 15g licorice, 20g skullcap, 4g dried alum, 20g honeysuckle, 50g emulsifier, 10g phosphoric acid.

[0021] Grind licorice, scutellaria baicalensis, dried alum, and honeysuckle, pass through a 20-40 mesh sieve, add 6-7 times of 30%-70% ethanol to the crushed matter to submerge them all, soak for 24-72 hours, and then infiltrate in a percolator , filter out larger particles, then heat the filtrate to evaporate residual ethanol, and concentrate to a solid-to-liquid ratio of 1:1, then centrifuge or use resin adsorption to filter out fine particles and other impurities, and the resulting filtrate is ready for use.

[0022] Mix iodine with an emulsifier, emulsify and complex into a paste, and set aside.

[0023] Mix the above-mentioned filtrate and paste, stir evenly, then add water to dilute, after stirring evenly, add medical phosphoric acid to adjust the pH to 1.3-2.8, and finally fill and seal to obtain the product.

Embodiment 3

[0025] Formula: 0.05g iodine, 15g licorice, 20g skullcap, 0.2g dried alum, 3g honeysuckle, 50g emulsifier, 10g phosphoric acid.

[0026] Grind licorice, scutellaria baicalensis, dried alum, and honeysuckle, pass through a 20-40 mesh sieve, add 6-7 times of 30%-70% ethanol to the crushed matter to submerge them all, soak for 24-72 hours, and then infiltrate in a percolator , filter out larger particles, then heat the filtrate to evaporate residual ethanol, and concentrate to a solid-to-liquid ratio of 1:1, then centrifuge or use resin adsorption to filter out fine particles and other impurities, and the resulting filtrate is ready for use.

[0027] Mix iodine with an emulsifier, emulsify and complex into a paste, and set aside.

[0028] Mix the above-mentioned filtrate and paste, stir evenly, then add water to dilute, after stirring evenly, add medical phosphoric acid to adjust the pH to 1.3-2.8, and finally fill and seal to obtain the product.

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PUM

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Abstract

The invention provides a preparation method of a sterilization medicament. The preparation method of the sterilization medicament is characterized in that liquorice, radix scutellariae, dried alum and honeysuckle are smashed, the mixture is screened with a sieve with the mesh numbers being 20-40, ethyl alcohol with the concentrate being 30%-70% is added to the smashed mixture to completely submerge the smashed mixture, the amount of the ethyl alcohol is 6-7 times that of the smashed mixture, and dipping is conducted for 24-72 h; then, the mixture is percolated in a percolator, large-sized particles are filtered off, obtained filter liquor is heated, residual ethyl alcohol is volatilized, and the obtained liquor is concentrated until the solid-to-liquid ratio is 1:1; centrifugal separation or resin adsorption is conducted, fine particles and other impurities are filtered off, and obtained filter liquor stands for use; iodine is mixed with an emulsifying agent, and a cream object is obtained through emulsification and complexation and stands for use; the filter liquor and the cream object are mixed and evenly stirred, water is added to the mixture for attenuation, and after even stirring, medical phosphoric acid is added to adjust the ph to be 1.3-2.8; and finally, the product is obtained after filling and sealing.

Description

technical field [0001] The invention belongs to the field of fine chemicals, and in particular relates to a method for preparing a bactericidal agent and a product prepared by the method. Background technique [0002] Chemical agents play an important role in the control of crop diseases and insect pests. However, due to the long-term use of chemical agents, the frequency of resistance to diseases and insect pests in most areas exceeds 50%, and the resistance level is as high as more than 10,000 times. The single use of chemical agents has completely lost the control effect. Moreover, with the continuous enhancement of resistant strains, the frequency of pesticide application has increased year by year, and the amount of pesticide application has also doubled, which has brought great pressure to the control and the surrounding environment. Its disadvantages are also becoming more and more prominent, such as drug residues, environmental pollution and harmful organisms rampant...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/539A61P31/02A61P1/02A61K33/06A61K33/18
CPCA61K36/484A61K33/06A61K33/18A61K36/355A61K36/539A61K2236/333A61K2236/51A61K2236/53A61K2236/55
Inventor 李海燕
Owner 李海燕
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