Bismaleimide resin/silicone rubber ablation-resistant thermal insulation composite material and preparation method thereof
A technology of Shuangma resin and composite materials, which is applied in the field of thermal protection of the afterburner chamber of the integral solid-impact engine, can solve the problems of poor oxidation resistance, easy cracks, poor elasticity, etc., and achieve high temperature resistance and flame retardancy. Improved ablation resistance and ease of handling
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Embodiment 1
[0027] Use silane coupling agent to carry out surface treatment to fumed white carbon black, zirconium boride and chopped carbon fiber, stand-by; Add 35 parts of methyl vinyl silicone rubber and 65 parts of methyl vinyl phenyl silicone rubber to the mixer Mixing at 80°C to a transparent state; add 2 parts of hydroxyl silicone oil, 25 parts of surface-treated fumed silica, 10 parts of surface-treated micron zirconium boride powder, and 15 parts of surface-treated average length of 9mm chopped carbon fiber continue to mix until evenly mixed; add 20 parts of double horse resin and 2 parts of dicumyl peroxide, continue to mix until evenly mixed; after mixing, take it out and let it stand for 25 hours; then according to the required thickness And size, sheet; two-stage vulcanization: one-stage vulcanization, pressure vulcanization, pressure is 12MPa, vulcanization temperature is 160°C, vulcanization time is 15min; two-stage vulcanization: normal pressure vulcanization, temperature i...
Embodiment 2
[0030] Use silane coupling agent to carry out surface treatment to fumed silica, zirconium boride and chopped carbon fiber, stand-by; add 30 parts of methyl vinyl silicone rubber and 70 parts of methyl vinyl phenyl silicone rubber to the mixer Mixing at 90°C to a transparent state; add 3 parts of hydroxyl silicone oil, 20 parts of surface-treated fumed silica, 15 parts of pretreated micron zirconium boride powder, and 10 parts of surface-treated average length of 10mm chopped carbon fiber continue to mix until evenly mixed; add 25 parts of Shuangma resin and 3 parts of dicumyl peroxide, continue to mix until evenly mixed; after mixing, take it out and let it stand for 28 hours; then according to the required thickness and size, sheet output; two-stage vulcanization: one-stage vulcanization, pressure vulcanization, pressure 15MPa, vulcanization temperature 180°C, vulcanization time 20min; two-stage vulcanization: normal pressure vulcanization, temperature 220°C, time 4h.
[003...
Embodiment 3
[0033] Use silane coupling agent to carry out surface treatment to fumed silica, zirconium boride and chopped carbon fiber, stand-by; add 20 parts of methyl vinyl silicone rubber and 80 parts of methyl vinyl phenyl silicone rubber to the mixer Mixing at 70°C to a transparent state; add 1 part of hydroxyl silicone oil, 15 parts of surface-treated fumed silica, 20 parts of pretreated micron zirconium boride powder, and 6 parts of surface-treated average length of 8mm chopped carbon fiber continue to mix until evenly mixed; add 5 parts of Shuangma resin and 1 part of dicumyl peroxide, continue to mix until evenly mixed; after mixing, take it out and let it stand for 15 hours; then according to the required thickness And size, sheet; two-stage vulcanization: one-stage vulcanization, pressure vulcanization, pressure 10MPa, vulcanization temperature 200°C, vulcanization time 25min; two-stage vulcanization: normal pressure vulcanization, temperature 200°C, time 2h.
[0034] The prepa...
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Abstract
Description
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Application Information
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