A kind of preparation technology of Ganoderma lucidum spore oil

A Ganoderma lucidum spore oil and preparation technology, which is applied in the field of preparation technology of Ganoderma lucidum spore oil, can solve the problems of incomplete retention, general quality of raw materials, and inability to retain active ingredients, so as to achieve clear and clear oil, low residual amount of extraction solvent, high cost effect

Active Publication Date: 2021-03-26
NANJING XIYUAN BIOPHARML SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the existing related technologies, although the subcritical extraction method is also used, the quality of the raw materials used is average, and the obtained Ganoderma lucidum spore oil product cannot completely retain its original characteristics in terms of color and taste.
In addition, the active ingredients in its products cannot be retained to the greatest extent

Method used

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  • A kind of preparation technology of Ganoderma lucidum spore oil
  • A kind of preparation technology of Ganoderma lucidum spore oil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Preparation of broken ganoderma lucidum spore powder:

[0026] (1) Raw material preparation: take the ganoderma lucidum spore powder raw material, wash with water, and remove impurities;

[0027] (2) Vacuum drying: set the vacuum degree and vacuum drying time, the vacuum degree is 0.9MPa, the vacuum drying time is 6h, so that the moisture after vacuum drying is ≤6%;

[0028] (3) Freeze embrittlement and wall breaking: place the vacuum-dried raw materials at -18°C for embrittlement for 4 hours; then at 55°C, carry out ultrasonic mixing to break the wall. The time is 8 minutes, the mixing speed is 35 rpm, and the broken ganoderma spore powder is obtained.

[0029] Preparation of ganoderma lucidum spore oil:

[0030] (1) Raw material granulation: take the above-mentioned broken ganoderma lucidum spore powder, add purified water to mix and granulate, the mass ratio of the broken ganoderma lucidum spore powder:purified water is=1:0.3; the granulation adopts a rotary granul...

Embodiment 2

[0036] Preparation of broken ganoderma lucidum spore powder:

[0037] (1) Raw material preparation: take the ganoderma lucidum spore powder raw material, wash with water, and remove impurities;

[0038] (2) Vacuum drying: set the vacuum degree and vacuum drying time, the vacuum degree is 0.9MPa, the vacuum drying time is 6h, so that the moisture after vacuum drying is ≤6%;

[0039] (3) Freeze embrittlement and wall breaking: place the vacuum-dried raw materials at -18°C for embrittlement for 4 hours; then at 55°C, carry out ultrasonic mixing to break the wall. The time is 8 minutes, the mixing speed is 35 rpm, and the broken ganoderma spore powder is obtained.

[0040] Preparation of ganoderma lucidum spore oil:

[0041] (1) Raw material granulation: take the above-mentioned broken ganoderma lucidum spore powder, add purified water to mix and granulate, the mass ratio of the broken ganoderma lucidum spore powder:purified water is=1:0.4; the granulation adopts a rotary granul...

Embodiment 3

[0047] Preparation of broken ganoderma lucidum spore powder:

[0048] (1) Raw material preparation: take the ganoderma lucidum spore powder raw material, wash with water, and remove impurities;

[0049] (2) Vacuum drying: set the vacuum degree and vacuum drying time, the vacuum degree is 0.9MPa, the vacuum drying time is 6h, so that the moisture after vacuum drying is ≤6%;

[0050] (3) Freeze embrittlement and wall breaking: place the vacuum-dried raw materials at -18°C for embrittlement for 4 hours; then at 55°C, carry out ultrasonic mixing to break the wall. The time is 8 minutes, the mixing speed is 35 rpm, and the broken ganoderma spore powder is obtained.

[0051] Preparation of ganoderma lucidum spore oil:

[0052] (1) Raw material granulation: take the above-mentioned broken ganoderma lucidum spore powder, add purified water to mix and granulate, the mass ratio of the broken ganoderma lucidum spore powder:purified water is =1:0.35; the granulation adopts a rotary granul...

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Abstract

The invention discloses a preparation process of ganoderma lucidum spores oil. The ganoderma lucidum spores oil is mainly prepared from the following steps of (1) taking broken wall ganoderma lucidum spores powder; adding purified water for mixed pelletization, wherein the mass ratio of the ganoderma lucidum spores powder to the purified water is 1:(0.3 to 0.4); (2) setting the air inlet temperature to be 45 to 60 DEG C, the air outlet temperature to be 35 to 45 DEG C and the flow rate to be (4500 to 5000)m<3> / hr; drying the particles obtained in the step (1) to obtain dry particles; (3) setting the pressure of an extraction device to be 5 to 8MPa and the temperature to be 35 to 40 DEG C; selecting butane as solvents; adding the butane into the dry particles for extraction; after the completion, performing separation to obtain crude oil; (4) performing still standing on the obtained crude oil for 20 to 30h; then, performing air pressure filtering; (5) setting the vacuum degree of an exsolution device to be -0.1 to -0.2MPa; maintaining the exsolution time to be 25 to 45 minutes; removing the solvents of butane; obtaining the ganoderma lucidum spores oil. Compared with the prior art, the preparation process provided by the invention has the advantages that the prepared ganoderma lucidum spores oil has transparent color and luster; the special flavor of the ganoderma lucidum spores oil is realized; in addition, the residue quantity can reach 1ppm.

Description

technical field [0001] The invention belongs to the technical field of extracting effective components of ganoderma lucidum spores, and in particular relates to a preparation process of ganoderma lucidum spore oil. Background technique [0002] Ganoderma lucidum spores are the germ cells of Ganoderma lucidum. The spores of Ganoderma lucidum are generally light brown to yellowish brown, oval, (8.5-11.2) μm × (5.2-6.9) μm, and contain oil droplets. Ganoderma lucidum spore oil is a lipid active substance extracted from Ganoderma lucidum spores, usually only 1g of Ganoderma lucidum spore oil can be extracted from 20g of Ganoderma lucidum spore powder. Ganoderma lucidum spore oil is rich in active ingredients such as triterpenoid ganoderma acid, unsaturated fatty acids, organic germanium, and ganoderma polysaccharides in ganoderma lucidum spores. Liver protection and other health benefits. [0003] At present, most Ganoderma lucidum spore oils on the market are prepared by carb...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B1/10C11B1/02
CPCC11B1/02C11B1/10C11B1/108
Inventor 刘勇业
Owner NANJING XIYUAN BIOPHARML SCI & TECH
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