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Method for producing nubia goat cholic acid

A technology of Nubian goat and goat cholic acid, which is applied in the production field of Nubian goat cholic acid, can solve problems such as complex methods and low production efficiency, achieve broad market prospects, low production cost, improve production efficiency and product quality quality effect

Inactive Publication Date: 2016-12-14
LIUZHOU CITY LIUNAN DISTRICT ANSHUN BREEDING ASSOCS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The existing production method of bovine and sheep cholic acid is complex and has low production efficiency

Method used

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Embodiment Construction

[0011] The technical solution of the present invention will be described in detail below.

[0012] In order to solve the above-mentioned problems existing in prior art and actual situation, the invention provides a kind of production method of Nubian goat cholic acid, it is characterized in that, comprises the following steps:

[0013] 1) Collect the bitter gall of fresh Nubian goats, cut the gall skin, collect the bile and filter it, stir evenly, add 0.1 times (10%) to the total weight of the bile, add sodium hydroxide (caustic soda, caustic soda) and stir and heat until Boil and melt for 24 hours, add water at any time during the melt;

[0014] 2) After the silk is melted, cool to room temperature, siphon the upper clear night, filter the lower precipitate with a cloth (combined filtrate) into another container, cool to below room temperature, then add 2-3% hydrogen peroxide and stir for 15 minutes, stand still Precipitate for 30 minutes;

[0015] 3) add acid to filter, st...

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PUM

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Abstract

The invention provides a method for producing nubia goat cholic acid. The method includes the steps that cholic skin is sheared, bile is collected, filtered and mixed to be even, 0.1 fold of the total weight of the bile is added, sodium hydroxide is added, the mixture is stirred, heated to be boiled and subjected to silk forming treatment for 24 hours, and clear water is supplemented at any moment during silk forming treatment; after silk forming treatment is completed, the mixture is cooled to be at the room temperature, supernatant liquid is siphoned and collected, lower-layer sediment is filtered with cloth into another container and cooled to be at the temperature lower than the room temperature, then hydrogen peroxide of 2% to 3% is added, the mixture is sufficiently stirred for 15 minutes, and standing precipitating is carried out for 30 minutes; acid is added into the mixture, and filtering, stirring and precipitating are carried out; after cholic acid floats to the liquid surface, floating substances are salvaged and placed into a pot, one fold of clear water and acetic ether is added, the mixture is stirred to be even and heated to be boiled for 30 minutes, the cholic acid forms particles, the particles are filtered, washed to be neutral with clear water and dried in a hung mode, and semi-finished nubia goat cholic acid is prepared; ethyl alcohol and hydrogen peroxide in the proportion of 100:(2-3) are mixed, the ethyl-alcohol and hydrogen-peroxide mixture is led into the semi-finished nubia goat cholic acid, and the mixture is stirred to be in a stirred-feed type and dried in a centrifugal machine.

Description

technical field [0001] The invention relates to the technical field of livestock breeding, in particular to a production method of Nubian goat cholic acid. Background technique [0002] In recent years, my country's animal husbandry has continued to develop at a high speed. Among cattle and sheep animals, bile acid exists in the bile of many vertebrates, and the bile of cattle, sheep and dogs is the most abundant, and it is used as a raw material for the preparation of artificial bezoar. The existing method for producing bovine and sheep cholic acid is complicated and has low production efficiency. Contents of the invention [0003] In order to solve the above-mentioned problems existing in prior art and actual situation, the invention provides a kind of production method of Nubian goat cholic acid, it is characterized in that, comprises the following steps: [0004] 1) Collect the bitter gall of fresh Nubian goats, cut the gall skin, collect the bile and filter it, stir ...

Claims

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Application Information

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IPC IPC(8): C07J9/00
CPCC07J9/005
Inventor 何以安
Owner LIUZHOU CITY LIUNAN DISTRICT ANSHUN BREEDING ASSOCS
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