Method for preparing butyl alcohol by using green soy bean straws
A straw and butanol technology, applied in the field of butanol preparation, can solve the problems of low butanol yield and incomplete fermentable sugar, and achieve the effect of low cost, less investment and significant environmental protection effect
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Embodiment 1
[0038] A method for preparing butanol by utilizing edamame stalks, comprising the following steps:
[0039] S1: Rinse the edamame stalks with 12% salt water for 2.5 hours, and then dry the edamame stalks at a temperature of 95-103°C until the water content is ≤10%, to obtain dry edamame stalks;
[0040] S2: crushing the dry edamame stalks prepared in step S1, and passing through a 150-mesh sieve to obtain edamame straw granules;
[0041] S3: Put the edamame straw particles prepared in step S2 into a microwave reactor, add solution A and mix evenly, heat to 62°C, pretreat at a stirring speed of 300r / min for 1.1h, then cool to room temperature and filter to prepare Obtain pretreated edamame straw particles; the solution A is a mixed solution of acetone, ethanol, ammonium phosphotungstate, the mass concentration of the acetone is 9%, the mass concentration of the ethanol is 70%, and the phosphotungstic The mass concentration of the acid ammonium salt is 7%, the volume ratio of t...
Embodiment 2
[0045] A method for preparing butanol by utilizing edamame stalks, comprising the following steps:
[0046] S1: Rinse the edamame stalks with 10% salt water for 3 hours, and then dry the edamame stalks at a temperature of 95-103°C until the water content is ≤10%, to obtain dry edamame stalks;
[0047] S2: crushing the dry edamame stalks prepared in step S1, and passing through a 120-mesh sieve to obtain edamame straw granules;
[0048] S3: Put the edamame straw particles prepared in step S2 into a microwave reactor, add solution A and mix evenly, heat to 60°C, pretreat at a stirring speed of 200r / min for 1.3h, then cool to room temperature and filter to prepare Obtain pretreated edamame straw particles; the solution A is a mixed solution of acetone, ethanol, ammonium phosphotungstate, the mass concentration of the acetone is 8%, the mass concentration of the ethanol is 60%, and the phosphotungstic The mass concentration of ammonium acid salt is 6%, the volume ratio of the ace...
Embodiment 3
[0052] A method for preparing butanol by utilizing edamame stalks, comprising the following steps:
[0053] S1: Rinse the edamame stalks with 15% salt water for 2 hours, and then dry the edamame stalks at a temperature of 95-103°C until the water content is ≤10%, to obtain dry edamame stalks;
[0054] S2: crushing the dry edamame stalks prepared in step S1, passing through a 200-mesh sieve to obtain edamame straw granules;
[0055] S3: Put the edamame straw particles prepared in step S2 into a microwave reactor, add solution A and mix evenly, heat to 64°C, pretreat at a stirring speed of 300r / min for 0.9h, then cool to room temperature and filter to prepare Obtain pretreated edamame stalk particles; the solution A is a mixed solution of acetone, ethanol, ammonium phosphotungstate, the mass concentration of the acetone is 10%, the mass concentration of the ethanol is 80%, and the phosphotungstic The mass concentration of the acid ammonium salt is 8%, the volume ratio of the ac...
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