Method for removing sediment in tar sand oil
A technology for oil sand oil and mud sand, which is applied in the direction of multi-stage series refining process treatment, etc., can solve the problems of limited cyclone separation strength and poor removal effect, and achieves promotion of aggregation and settlement, improved production efficiency, and short cycle time. Effect
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Embodiment 1
[0011] Mix 50g of oil sand oil with 50g of naphtha and stir for 10min at a temperature of 30°C to fully dilute the asphalt. After the stirring is finished, add 25g of compound reagent prepared by calcium chloride and hydrochloric acid to the mixed oil, the mass fraction of hydrochloric acid in the compound reagent is 1%, the mass fraction of calcium chloride is 0.1%, stir at a temperature of 30°C The time is 10 minutes, and the sedimentation is 20 minutes. The sample is layered, the upper layer is purified mixed oil, and the lower layer is sediment. The upper mixed oil is distilled to recover diluent naphtha and obtain purified bitumen. Determination of the content of mechanical impurities such as sediment in purified asphalt. The removal rate of mechanical impurities is 95.2%.
Embodiment 2
[0013] Mix 50g of oil sand oil with 5g of toluene and stir for 10min at a temperature of 70°C to fully dilute the asphalt. After the stirring is finished, add 15g of compound reagent prepared by calcium nitrate and nitric acid to the mixed oil. The mass fraction of nitric acid in the compound reagent is 10%, and the mass fraction of calcium nitrate is 2%. 10 minutes, settling for 20 minutes, the sample is separated, the upper layer is purified mixed oil, and the lower layer is sediment. Distill the mixed oil in the upper layer to recover the diluent toluene and obtain purified asphalt. Determination of the content of mechanical impurities such as sediment in purified asphalt. The removal rate of mechanical impurities is 97.5%.
Embodiment 3
[0015] Take 50g oil sand oil and 25g 120 # Mix with solvent oil and stir for 10 minutes at a temperature of 100°C to fully dilute the asphalt. After the stirring is finished, add 5g of compound reagent prepared by magnesium chloride and formic acid to the mixed oil, the mass fraction of formic acid in the compound reagent is 20%, the mass fraction of magnesium chloride is 5%, and the stirring time is 10min at a temperature of 100°C. After settling for 20 minutes, the samples were layered, the upper layer was purified mixed oil, and the lower layer was sediment. The upper layer mixed oil is distilled, and the diluent 120 is recovered # mineral spirits, while getting purified bitumen. Determination of the content of mechanical impurities such as sediment in purified asphalt. The removal rate of mechanical impurities is 95.8%.
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