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Preparation method of high efficient and energy saving phenolic foam board

A phenolic foam board, high-efficiency and energy-saving technology, applied in sustainable manufacturing/processing, chemical industry, climate sustainability, etc., can solve problems such as reducing flame retardant effect, and achieve the effect of increasing closed cell rate and reducing thermal conductivity

Inactive Publication Date: 2016-07-06
苏州美克思新能源科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, once the flame retardant material is ablated by this layered insulation board, the flame retardant effect will be greatly reduced in the subsequent process.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A preparation method of a high-efficiency and energy-saving phenolic foam board adopts the following steps:

[0020] (1) Prepare materials according to the following components and parts by weight: expandable resole phenolic resin 100, foaming agent 2, flame retardant 5, foam stabilizer 2, curing agent 10, wherein expandable resole phenolic resin The water content of the product is controlled at 5-8wt%, the viscosity is controlled at 12000-18000cps, and the blowing agent is a mixture of n-pentane and isopentane ， Its boiling point is 30-31°C, the flame retardant is aluminum hydroxide with a particle size ≥ 1200 mesh, the foam stabilizer is a mixture of dimethyl silicone oil and Tween 80, each with a mass content of 50%, and the curing agent is p-toluenesulfonic acid , phenolsulfonic acid, sulfuric acid, phosphoric acid, and water are mixed in a weight ratio of 30:40:20:20:30;

[0021] (2) Stir evenly under the high-speed mixer after above-mentioned raw material is mixe...

Embodiment 2

[0024] A preparation method of a high-efficiency and energy-saving phenolic foam board adopts the following steps:

[0025] (1) Prepare materials according to the following components and parts by weight: expandable resole phenolic resin 100, foaming agent 4, flame retardant 10, foam stabilizer 3, curing agent 15, wherein, expandable resole phenolic resin The water content of the product is controlled at 5-8wt%, the viscosity is controlled at 12000-18000cps, the foaming agent is a mixture of n-pentane and isopentane, its boiling point is 30-31°C, and the flame retardant is aluminum hydroxide with particle size ≥ 1200 mesh , the foam stabilizer is a mixture of simethicone oil and Tween 80 in a weight ratio of 1:1, and the curing agent is p-toluenesulfonic acid, phenolsulfonic acid, sulfuric acid, phosphoric acid, water in proportion: 35:40:20: 20:35 mixed;

[0026] (2) Stir evenly under the high-speed mixer after above-mentioned raw material is mixed, then pour in the mould, m...

Embodiment 3

[0029] A preparation method of a high-efficiency and energy-saving phenolic foam board adopts the following steps:

[0030] (1) Prepare materials according to the following components and parts by weight: expandable resole phenolic resin 100, foaming agent 6, flame retardant 15, foam stabilizer 4, curing agent 20, wherein, expandable resole phenolic resin The water content of the product is controlled at 5-8wt%, the viscosity is controlled at 12000-18000cps, the foaming agent is a mixture of n-pentane and isopentane, its boiling point is 30-31°C, and the flame retardant is silica with particle size ≥ 1200 mesh , the foam stabilizer is a mixture of simethicone oil and Tween 80 in a weight ratio of 1:1, and the curing agent is p-toluenesulfonic acid, phenolsulfonic acid, sulfuric acid, phosphoric acid, water in proportion: 40:40:20: 20:40 mixed;

[0031] (2) Stir evenly under the high-speed mixer after above-mentioned raw material is mixed, then pour in the mould, mold is seale...

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Abstract

The invention relates to a preparation method of a high efficient and energy saving phenolic foam board, which includes the steps of: (1) preparing raw materials according to the following components and weight parts: 100 parts of expandable resol resin, 2-6 parts of a foaming agent, 5-15 parts of a fire retardant, 2-4 parts of a foam stabilizer, and 10-20 parts of a curing agent; (2) mixing above raw materials and stirring infirmly the raw materials at the high speed, pouring the raw materials into a die, sealing the die, and putting the die into a baking oven; and (3) controlling the temperature of the baking oven, carrying out staging foaming treatment on the die at different temperatures, taking out the die after the staging foaming treatment ends, namely preparing the high efficient and energy saving phenolic foam board. Compared with the prior art, the prepared product accords with high efficient, energy saving, and light characteristics. The thermal conduction coefficient may be low to 0.022W / m*K.

Description

technical field [0001] The invention relates to the field of thermal insulation materials for external walls, in particular to a method for preparing a high-efficiency and energy-saving phenolic foam board. Background technique [0002] With the continuous occurrence of fires of external wall insulation materials, more and more researches have been done on the use of external wall insulation materials in construction projects. Among many thermal insulation materials, phenolic foam foamed from phenolic resin is known as the "king of thermal insulation" as a new type of thermal insulation material. At the same time, it has the advantages of fire resistance, corrosion resistance, and environmental protection, and has been widely used abroad. Many countries specify that architectural design prefers phenolic foam as a building thermal insulation material. Because domestic research on phenolic foam started relatively late, many properties are far below foreign levels, so the use ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L61/06C08K13/02C08K3/22C08K3/36C08K5/42C08K3/30C08K3/32C08J9/14
CPCY02P20/10
Inventor 杨金平薛永顺
Owner 苏州美克思新能源科技有限公司
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