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Preparation method and application of cross-linked resin for spinning

A cross-linking resin and textile technology, applied in textiles and papermaking, shrink-resistant fibers, fiber processing, etc., can solve the problems of the decline of color and brightness of the cloth surface, and improve the color, clear texture and bright color of the cloth surface. Effect

Inactive Publication Date: 2016-05-04
中山市巴斯基纺织助剂有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] After the use of traditional resin, it is difficult to carry out reverse work and color correction treatment, and the color and brightness of the treated cloth surface have decreased to varying degrees, so it is urgently needed

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Add 1456kg of glyoxal to the reaction kettle and use triethanolamine to adjust PH=5, add 588kg urea, react for 30min, use 25% pure lye, adjust PH=8–8.5 and raise the temperature to 45-550°C, keep the temperature for 3 hours, and cool down to 400°C, add 1456kg formaldehyde, use 25% soda ash to adjust PH=8–8.5, raise the temperature to 45–550°C, keep warm for 3 hours, add 1092kg methanol, etherify for 2 hours, add 16.8kg self-made bleaching aid, 840kg Water, modified for 1 hour, can be discharged.

Embodiment 2

[0025] Add 1456kg of glyoxal to the reaction kettle and use triethanolamine to adjust PH=5, add 588kg urea, react for 30min, use 25% pure lye, adjust PH=8–8.5 and raise the temperature to 45-550°C, keep the temperature for 3 hours, and cool down to 400℃, add 1456kg formaldehyde, adjust PH=8-8.5 with 25% soda ash, raise the temperature to 45-550℃, keep warm for 3 hours, add 1092kg ethanol, etherify for 2 hours, add 16.8kg self-made bleaching aid, 840kg Water, modified for 1 hour, can be discharged.

Embodiment 3

[0027] Add 1456kg of glyoxal to the reaction kettle and use triethanolamine to adjust PH=5, add 588kg urea, react for 30min, use 25% pure lye, adjust PH=8–8.5 and raise the temperature to 45-550°C, keep the temperature for 3 hours, and cool down to 400°C, add 1456kg formaldehyde, use 25% soda ash to adjust PH=8–8.5, heat up to 45–550°C, keep warm for 3 hours, add 1092kg ethylene glycol, etherify for 2 hours, add 16.8kg self-made bleaching aid , 840kg of water, modified for 1 hour, then the material can be discharged.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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PUM

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Abstract

The invention provides a preparation method of cross-linked resin for spinning. The preparation method comprises the following steps: carrying out a cyclization reaction on glyoxal and urea, thus obtaining a reaction solution; enabling the reaction solution to react with formaldehyde, and generating first condensate; carrying out an etherification reaction on the first condensate and an etherifying agent; finally modifying by adding a bleaching agent and water. The invention also provides the application of the cross-linked resin for spinning. The application comprises the following steps: selecting the cross-linked resin prepared by the preparation method; drying the cross-linked resin under the action of a catalyst when the temperature is 60 DEG C to 80 DEG C; baking under 145 DEG C after carrying out pressing and forming on fabric. According to the cross-linked resin prepared by using the preparation method, free formaldehyde on the surface of a cloth cover is low; meanwhile, by using the cross-linked resin, not only can original characteristics of a product be kept, but also the color of the cloth cover is increased, the color is fresher, the grains are clearer, and the cross-linked resin can be used for special technology, reworking and shading treatment of the cloth cover.

Description

technical field [0001] The invention relates to a resin and its application, in particular to a preparation method and application of a cross-linked resin for textile use. Background technique [0002] In the 1930s, people began to study anti-wrinkle and anti-shrinkage finishing agents because of the obvious wrinkling and shrinkage deformation of fabrics during the washing process. After decades, anti-wrinkle and anti-shrinkage treatment has become one of the important processes in textile dyeing and finishing. So far, dozens of varieties have been developed, such as: urea-formaldehyde resin initial shrinkage body, hexamethylolmelamine formaldehyde resin, Initial contraction body of dimethylol dihydroxyethyl ethylene urea resin, initial contraction body of dimethylol triazone resin, etc. With the improvement of people's living standards and the enhancement of environmental protection awareness, reducing the release of formaldehyde and functional products have become the goa...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08G12/42C08G12/12D06M15/423
CPCC08G12/422C08G12/12D06M15/423D06M2200/20D06M2200/45
Inventor 刘险锋
Owner 中山市巴斯基纺织助剂有限公司
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