A kind of modified hindered phenol damping agent and its preparation method and application
A hindered phenol and damping agent technology, applied in the field of damping materials, can solve the problems of long-term maintenance and easy migration that affect the damping effect, and achieve the effects of enhancing compatibility, overcoming easy migration, and broad application prospects
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0034] 1. Preparation of N,N-dihydroxyethyl-3-aminopropionic acid methyl ester monomer:
[0035] Add 0.2mol methyl acrylate, 0.4mol diethanolamine and 20mL methanol into the three-necked flask, 2 Stir and react at 20°C for 50 minutes under protection, then raise the temperature to 30°C and keep it warm for 6 hours, then end the reaction, vacuumize to remove excess methanol solvent, and obtain a colorless and transparent oily substance, which is: N,N-dihydroxyethyl- Methyl 3-aminopropionate monomer.
[0036] 2. Preparation of modified hindered phenol damping agent:
[0037] Take by weighing 50g of BASF Antioxidant 1010, 80g of the N,N-dihydroxyethyl-3-aminopropionic acid methyl ester monomer and 0.5g of p-toluenesulfonic acid prepared in the above steps in a four-necked flask, in N 2 Under protection, the reaction was stirred at 110°C for 7 hours, and then vacuumized to remove unreacted N,N-dihydroxyethyl-3-aminopropionic acid methyl ester monomer, and the resulting residue w...
Embodiment 2
[0039] 1. Preparation of N,N-dihydroxyethyl-3-aminopropionic acid methyl ester monomer:
[0040] Add 0.3mol methyl acrylate, 0.6mol diethanolamine and 25mL methanol into the three-necked flask, 2 Stir and react at 25°C for 45 minutes under protection, then raise the temperature to 40°C and keep the temperature for 5 hours, then end the reaction, vacuumize to remove excess methanol solvent, and obtain a colorless and transparent oil, which is: N,N-dihydroxyethyl- Methyl 3-aminopropionate monomer.
[0041] 2. Preparation of modified hindered phenol damping agent:
[0042] Take by weighing 65g of BASF Antioxidant 1076, 90g of the N,N-dihydroxyethyl-3-aminopropionic acid methyl ester monomer and 0.6g of p-toluenesulfonic acid prepared in the above steps in a four-necked flask, in N 2 Under protection, the reaction was stirred at 100°C for 8 hours, and then vacuumized to remove unreacted N,N-dihydroxyethyl-3-aminopropionic acid methyl ester monomer, and the resulting residue was ...
Embodiment 3
[0044] 1. Preparation of N,N-dihydroxyethyl-3-aminopropionic acid methyl ester monomer:
[0045] Add 0.4mol methyl acrylate, 0.8mol diethanolamine and 30mL methanol into the three-necked flask, 2 Stir and react at 30°C for 40min under protection, then raise the temperature to 50°C and keep it warm for 4h, then end the reaction, vacuumize to remove excess methanol solvent, and obtain a colorless and transparent oily substance, which is: N,N-dihydroxyethyl- Methyl 3-aminopropionate monomer.
[0046] 2. Preparation of modified hindered phenol damping agent:
[0047] Take by weighing 80g of BASF Antioxidant 1076, 100g of the N,N-dihydroxyethyl-3-aminopropionic acid methyl ester monomer and 0.8g of p-toluenesulfonic acid prepared in the above steps in a four-necked flask, in N 2 Under protection, the reaction was stirred at 110°C for 7 hours, and then vacuumized to remove unreacted N,N-dihydroxyethyl-3-aminopropionic acid methyl ester monomer, and the resulting residue was washed...
PUM
Property | Measurement | Unit |
---|---|---|
Branching factor | aaaaa | aaaaa |
molecular weight distribution | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com