Ionization method and ionization device
An ionization and ion source technology, applied in the field of mass spectrometry, can solve problems such as complex sample analysis steps, and achieve the effects of wide application range, easy implementation, and remarkable practicability
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Embodiment 1
[0070] Will figure 1 The flame ionization device shown is combined with a mass spectrometer (the mass analyzer is Fourier transform ion cyclotron resonance), and for the liquid sample methyl salicylate (Methylsalicylate, MW=152): Perform mass spectrometry:
[0071] Use n-butane as fuel to make it burn to produce flame 1;
[0072] Spray a sample of methyl salicylate over or around the flame;
[0073] Keep the flame burning continuously, and the mass analyzer is always in the collection state;
[0074] image 3 For the mass spectrum obtained by image 3 The mass spectrum shown can be seen: the ion peak related to methyl salicylate appears in the spectrum [M+H] + =153, indicating that the device and method of the present invention can achieve good ionization efficiency.
Embodiment 2
[0076] Will figure 1 The ionization device shown is combined with a mass spectrometer (the mass analyzer is Fourier transform ion cyclotron resonance), and for the liquid sample dimethyl sulfoxide (Dimethylsulfoxide, MW=78): Perform mass spectrometry:
[0077] Use n-butane as fuel to make it burn to produce flame 1;
[0078] Keep containers of DMSO open near flames;
[0079] Keep the flame burning continuously, and the mass analyzer is always in the collection state;
[0080] Figure 4 For the mass spectrum obtained by Figure 4 The mass spectrum shown can be seen: the ion peak related to dimethyl sulfoxide appears in the spectrum [2M+H] + =157, indicating that the device and method of the present invention can achieve good ionization efficiency.
Embodiment 3
[0082] Will figure 1 The ionization device shown is combined with a mass spectrometer (the mass analyzer is Fourier transform ion cyclotron resonance), and for the liquid sample diethylene glycol dimethyl ether (2-Methoxyethylether, MW=134): Perform mass spectrometry:
[0083] Use n-butane as fuel to make it burn to produce flame 1;
[0084] Keep the container of diethylene glycol dimethyl ether open near the flame;
[0085] Keep the flame burning continuously, and the mass analyzer is always in the collection state;
[0086] Figure 5 For the mass spectrum obtained by Figure 5 The mass spectrum shown can be seen: the ion peak [M+H] related to diethylene glycol dimethyl ether appears in the spectrum + =135, indicating that the device and method of the present invention can achieve good ionization efficiency.
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