Supercritical extraction method for peony seed essential oil
The technology of peony seed essential oil and peony seed is applied in the directions of essential oil/spice, fat production, etc., and can solve the problems of low quality of essential oil, long extraction time and high production cost, and achieves simple process, convenient operation, prevention of oxidation and escape. scattered effect
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Embodiment 1
[0015] Step 1: remove impurities from the peony seeds, put them into the sieving equipment, put the sieved peony seeds into the drying equipment, heat them to 66°C, dry them for 18 hours, put them into the crushing equipment, crush them and sieve them to obtain 65 mesh peony seeds scrap, spare;
[0016] Put 280kg peony seed fragments into the extraction kettle and start the extraction. The extraction temperature is 50°C, the extraction pressure is 27Mpa, and the extraction time is 145min. Close the extractor, check to ensure that it is tightly sealed, and use a high-pressure pump to remove the liquid CO2 in the storage tank. Pump into the vaporizer, gasify into a critical fluid state, and then enter the extractor to extract the peony seed fragments. Set the pressure in the extractor to 18Mpa and the temperature to 38°C. The mixed fluid of extracted CO2 and peony seed essential oil Enter the separator for decompression separation, the carbon dioxide flow rate is 27kg / h, the pre...
Embodiment 2
[0020] Step 1: remove impurities from the peony seeds, put them into the sieving equipment, put the sifted peony seeds into the drying equipment, heat them to 77°C, dry them for 10 hours, put them into the crushing equipment, crush them and sieve them to obtain 60 mesh peony seeds scrap, spare;
[0021] Put 380kg peony seed fragments into the extraction kettle and start the extraction. The extraction temperature is 47°C, the extraction pressure is 26Mpa, and the extraction time is 145min. Close the extractor, check to ensure that it is tightly sealed, and use a high-pressure pump to remove the liquid CO2 in the storage tank. Pump into the vaporizer, gasify into a critical fluid state, and then enter the extractor to extract the peony seed fragments. Set the pressure in the extractor to 13Mpa and the temperature to 38°C. The mixed fluid of extracted CO2 and peony seed essential oil Enter the separator for decompression separation, the carbon dioxide flow rate is 27kg / h, the pre...
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