A composite piezoelectric material prepared from piezoceramic powder, carbon black and asphalt and a preparing method thereof
A technology of piezoelectric ceramics and piezoelectric materials is applied in the field of preparation of composite piezoelectric materials, which can solve the problems of reducing the degree of polarization of ceramics, increasing dielectric loss, insufficient polarization, etc., so as to improve the interface compatibility, The effect of improving piezoelectric performance and durable aging resistance
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specific Embodiment approach 1
[0023] (1) Raw materials are prepared in proportions by weight of 25-60 parts of asphalt, 2-5 parts of carbon black, 320-630 parts of piezoelectric ceramic powder and 1-10 parts of asphalt modifier.
[0024] (2) Pretreatment of piezoelectric ceramic powder: disperse 320 to 630 parts of piezoelectric ceramic powder and 2 to 5 parts of carbon black in step (1) in ethanol solution at 70°C, and then continuously stir in a magnetic stirrer until all the ethanol solution evaporated.
[0025] (3) Mixing of asphalt and modifier: put the asphalt in step (1) into a mold and heat to 170° C., then add the asphalt modifier in step (1) and stir for 5 minutes at a speed of 140 rpm.
[0026] (4) Mixing: Add the mixture of piezoelectric ceramic powder and carbon black obtained in step (2) and the mixture of asphalt and modifier obtained in step (3) and stir for 3 minutes at a stirring speed of 150 rpm to obtain a mixed material.
[0027] (5) Preheating the mold: put the mold into a drying ove...
specific Embodiment approach 2
[0033]This embodiment is based on Embodiment 1, and the asphalt is one or a mixture of petroleum asphalt and natural asphalt. Others are the same as the first embodiment.
[0034] When the asphalt described in this embodiment is a mixture, each component is mixed in any ratio.
specific Embodiment approach 3
[0035] This embodiment is based on the specific embodiment 1 or 2, and the piezoelectric ceramic powder is one or a mixture of lead-containing piezoelectric ceramic powder and lead-free piezoelectric ceramic powder. Others are the same as those in Embodiment 1 or 2.
[0036] The particle size of the piezoelectric ceramic powder in this embodiment is 0.5 μm to 70 μm, and the piezoelectric ceramic powder with a particle size of 0.5 μm to 2 μm and the piezoelectric ceramic powder with a particle size of 50 μm to 70 μm The volume ratio of powder is (0~5):1 mixture.
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