Preparation method of siraitia grosvenorii compound capsules
A Luo Han Guo and compound technology, which is applied in the field of preparation of plant extract compound capsules, can solve the problems of wasting Luo Han Guo resources, difficulty in concentration and spray drying, etc., and achieve the effect of novel combination technology, stable basic active ingredients, and prolonging the service life
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Embodiment 1
[0044] The first part of the preparation of Luo Han Guo compound extract
[0045] 1. Preliminary extraction of Luo Han Guo
[0046]Put the fresh Luo Han Guo in 6 times its quality of pure water to decoct to obtain Luo Han Guo residue and water extract A; place the Luo Han Guo residue in 8 times its quality of pure water for decoction to obtain water extract B; A and B are combined and filtered to obtain the initial extract of Luo Han Guo;
[0047] 2. Separation of mogrosides
[0048] Concentrate the initial extract of Luo Han Guo under reduced pressure to obtain a concentrated liquid; filter the concentrated liquid with a plate and frame to obtain a clear liquid of the concentrated liquid; absorb and decolorize the clear liquid of the concentrated liquid of Luo Han Guo with D101 styrene copolymer macroporous resin; recover Luo Han Guo effluent;
[0049] 3. Use the grosvenor fruit effluent as a solvent for extraction
[0050] Weigh 200kg of qualified dried tea leaves, 100kg...
Embodiment 2
[0066] The first part, the preparation of Luo Han Guo compound extract
[0067] 1. Use the grosvenor fruit effluent as a solvent for extraction.
[0068] Weigh 10kg of qualified dry tea leaves, 2.5kg of dried aloe leaves, and 5.0kg of dried hibiscus flowers as raw materials; use 100kg of Luo Han Guo effluent as a solvent, and extract in a 500L extraction tank. First heat to 90°C, and then turn on the auxiliary ultrasonic wave for extraction. After 6 hours, the extraction ends. After the extraction is completed, the extract is separated from the dregs through a vibrating sieve; then the extract is cooled to 50°C.
[0069] 2. Enzymolysis, decolorization, filtration and sterilization.
[0070] Weigh 20g of pectinase, 100g of papain, and 50g of cellulase, add them to 100kg of extract, and carry out enzymatic hydrolysis at a temperature of 45°C for 20 minutes; then add 50g of powdered activated carbon and keep warm for 40 minutes , to decolorize; then filter with a diatomite fil...
Embodiment 3
[0083] 1. Use the grosvenor fruit effluent as a solvent for extraction.
[0084] Weigh 2kg of qualified dry tea leaves, 2kg of dried aloe vera leaves, 1.5kg of dried hibiscus flowers, and 1.0kg of dried basil as raw materials; use 60kg of monk fruit effluent as solvent, extract in a 100L extraction tank, first heat to 70°C, and carry out Extract for 4 hours. After the extraction is completed, the extract is separated from the dregs by a residue-liquid separator; then the extract is cooled to 50°C.
[0085] Then use 60kg of Luo Han Guo effluent as a solvent, and repeat the extraction 2 times. Combine the cooled extracts.
[0086] 2. Enzymolysis, decolorization, filtration and sterilization.
[0087] Weigh 15g of pectinase, 120g of protease, and 80g of cellulase, add them to 50kg of extract, and carry out enzymatic hydrolysis. The temperature is controlled at 50°C for 30 minutes; Decolorization; then filter with a diatomite filter; use diatomite as a filter aid to first obta...
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