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Method for decoloring methionine crystallization mother liquor by adopting membrane integration technology

A technology for crystallization mother liquor and technical treatment, applied in the preparation of organic compounds, organic chemistry, chemical instruments and methods, etc., can solve the problems of reducing the efficiency of multi-effect evaporation, harsh production environment, large amount of activated carbon, etc. The effect of improving market competitiveness and reducing environmental pressure

Inactive Publication Date: 2015-08-19
HANGZHOU BLUETEC ENVIRONMENTAL TECH
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  • Abstract
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  • Claims
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Problems solved by technology

However, the disadvantages of this process are as follows: 1. The methionine crystallization mother liquor contains a large amount of pigment, which greatly reduces the efficiency of multi-effect evaporation, MVR and reverse osmosis membrane concentration; Large; 3. The decolorization of activated carbon leads to harsh production environment and serious dust pollution. The decolorized activated carbon becomes waste solids and needs outsourcing treatment

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  • Method for decoloring methionine crystallization mother liquor by adopting membrane integration technology

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Embodiment Construction

[0021] With reference to the accompanying drawings, the process of using membrane integration technology to process the methionine crystallization mother liquor provided by the present invention, the pH of the methionine crystallization mother liquor is between 3-5, and contains 2-5% methionine in the feed liquid, and the process has no effect on the methionine crystallization mother liquor. Carry out the following steps in turn:

[0022] 1), ultrafiltration system treatment (UF);

[0023] 2) Nanofiltration membrane decolorization and purification system treatment (NF); the nanofiltration concentrated liquid is washed and filtered with pure water and then directly transported to the incinerator for incineration, and the permeated liquid of the nanofiltration directly enters the subsequent multi-effect evaporation, MVR, reverse osmosis membrane concentration Wait for the follow-up process, and the concentrated solution returns to crystallization.

[0024] The recovery rate of ...

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Abstract

The invention provides a method for decoloring a methionine crystallization mother liquor by adopting a membrane integration technology. The method comprises the following steps: 1, carrying out ultrafiltration (UF) system treatment on methionine; and 2, carrying out nanofiltration (NF) membrane decoloring purification system treatment, adding pure water to the obtained nanofiltration concentrate, carrying out filter washing, directly conveying the obtained substance to a burning device, burning, and allowing an NF permeation liquid to directly enter a subsequent process. The clean production membrane integration decoloring technology is adopted to substitute active carbon decoloring in order to remove colloids and other pigments in the methionine crystallization mother liquor, so the generation of solid wastes of an enterprise is reduced, and the working environment of a decoloring workshop is improved; and high concentration multiple of the membrane technology is used, so the emission amount of wastewater is reduced, and the running pressure of the wastewater treatment station of the enterprise is reduced.

Description

technical field [0001] The invention relates to a process for decolorizing methionine crystallization mother liquor by membrane integration technology. Background technique [0002] Methionine, also known as methionine, is one of the essential amino acids that constitute the human body and participates in protein synthesis. Because it cannot be produced in the body itself, it must be obtained from the outside. If the lack of methionine will lead to blockage of protein synthesis in the body, resulting in damage to the body. Excessive oxidation of membrane lipids caused by oxygen free radicals in the body is the cause of various damages in the body. Lipid peroxides can damage the primary and secondary lysosomal membranes, release the hydrolyzed acid phosphatase contained in the lysosomes, and cause damage to important organelles such as cells and mitochondrial membranes. Methionine passes through a variety of ways to combat these damages. In recent years, the demand for me...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C323/58C07C319/28
Inventor 楼永通陈良易资利
Owner HANGZHOU BLUETEC ENVIRONMENTAL TECH
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