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Method for detecting quality of traditional Chinese medicine composition for treating anemopyretic cold

A quality inspection method and composition technology, which can be applied to drug combinations, pharmaceutical formulations, measuring devices, etc., and can solve problems such as inability to accurately control product quality.

Active Publication Date: 2015-07-01
ZHANGZHOU PIEN TZE HUANG PHARM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the original preparation standard of this traditional Chinese medicine composition only has the microscopic identification of honeysuckle, which cannot accurately control the product quality.

Method used

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  • Method for detecting quality of traditional Chinese medicine composition for treating anemopyretic cold
  • Method for detecting quality of traditional Chinese medicine composition for treating anemopyretic cold
  • Method for detecting quality of traditional Chinese medicine composition for treating anemopyretic cold

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0182] Embodiment 1 tablet preparation

[0183] [Prescription] Honeysuckle 234g, Vitex root 390g, Guanzhong 234g, Sanchaku 234g, gourd tea 234g, licorice 234g, peppermint oil 2ml.

[0184] [Preparation method] The above seven flavors, except peppermint oil, honeysuckle are crushed into fine powder, and the rest of Vitex root, Guanzhong, Sanchaku, gourd tea and licorice are decocted twice, adding 10 times the amount of water for the first time, decocting Boil for 2 hours, add 8 times the amount of water for the second time, decoct for 1 hour, combine the decoction liquid, filter, and condense the filtrate into a thick paste (d=1.15-1.25, 95°C), add the above honeysuckle fine powder and appropriate amount of auxiliary materials , made into granules, dried, sprayed with peppermint oil, mixed evenly, pressed into tablets, and obtained.

[0185] [Detection method] includes the following steps:

[0186] A. TLC identification of vitex root

[0187] Take 5g of the tablet, add 40ml ...

Embodiment 2

[0196] Embodiment 2 tablet preparation

[0197] [Prescription] Honeysuckle 240g, Vitex root 420g, Guanzhong 240g, Sanchaku 240g, Gourd Tea 240g, Licorice 240g, Peppermint Oil 4ml.

[0198] [Preparation method] The above seven flavors, except peppermint oil, honeysuckle are crushed into fine powder, and the rest of Vitex root, Guanzhong, Sanchaku, gourd tea and licorice are decocted twice, adding 6 times the amount of water for the first time, decocting Boil for 2 hours, add 10 times the amount of water for the second time, decoct for 1 hour, combine the decoction liquid, filter, and concentrate the filtrate into a thick paste (d=1.15-1.25, 95°C), add the above-mentioned honeysuckle fine powder and appropriate amount of auxiliary materials , made into granules, dried, sprayed with peppermint oil, mixed evenly, pressed into tablets, and obtained.

[0199] [Detection method] described detection method comprises the steps:

[0200] B. TLC identification of trigeminal bitter

[...

Embodiment 3

[0211] The preparation of embodiment 3 granules

[0212] [Prescription] Honeysuckle 220g, Vitex root 380g, Guanzhong 220g, Sanchaku 220g, gourd tea 220g, licorice 220g, peppermint oil 2ml.

[0213] [Preparation method] The above seven flavors, except peppermint oil, honeysuckle are crushed into fine powder, and the rest of Vitex root, Guanzhong, Sanchaku, gourd tea and licorice are decocted twice, adding 10 times the amount of water for the first time, decocting Boil for 2 hours, add 8 times the amount of water for the second time, decoct for 1 hour, combine the decoction liquid, filter, and concentrate the filtrate into a thick paste (d=1.15-1.25, 95°C), add the above honeysuckle fine powder and appropriate amount of auxiliary materials , made into granules, dried, sprayed with peppermint oil, and conventionally obtained granules.

[0214] [Detection method] described detection method comprises the steps:

[0215] A. TLC identification of vitex root

[0216] Take 10g of th...

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Abstract

The invention belongs to the field of Chinese medicine preparations and in particular relates to a method for detecting the quality of a traditional Chinese medicine composition for treating anemopyretic cold. According to the quality detection method, a TLC method is adopted for qualitatively identifying root of hempleaf Negundo chastetree, evodia lepta, Mussaenda pubescens and mint oil in a prescription, and the TLC method is adopted for qualitatively identifying honeysuckle in the prescription and / or a HPLC method is adopted for detecting the content of chlorogenic acid alternatively. The method has high accuracy, high sensitivity and a wide detection range, and the drug quality can be effectively controlled; and the method can be used as a conventional method for detecting the quality of the pharmaceutical preparations after being proofed by experiments.

Description

technical field [0001] The invention belongs to the field of traditional Chinese medicine preparations, and in particular relates to a quality detection method of a traditional Chinese medicine composition for treating anemopyretic cold. Background technique [0002] Traditional Chinese medicine is classified according to symptoms and physical reactions, and can be roughly divided into "wind-cold cold" and "wind-heat cold". Symptoms of wind-heat cold include: aversion to cold and fever, nasal congestion and runny nose (thick, yellow-green), thick phlegm, or accompanied by head and body pain, cough, sore throat, etc. Analysis of its pathogenesis shows that wind-heat pathogens mostly invade the human body through the mouth and nose, and its initial manifestation is superficial heat. Because the sun dominates the surface, the sun meridian is not good for transmission, and Wei Qi fights against it, and Wei Yang Qi cannot flow out smoothly, so there are symptoms of lung health s...

Claims

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Application Information

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IPC IPC(8): G01N30/90G01N30/88A61K36/85A61P11/00
Inventor 庄毅超林小红彭军徐伟李煌洪振丰
Owner ZHANGZHOU PIEN TZE HUANG PHARM
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