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Cinnamomum burmannii flower volatile oil effective component identification method

A technology of active ingredients and volatile oil, applied in the field of drug analysis, can solve problems such as unreported

Active Publication Date: 2015-06-24
SHIJIAZHUANG YILING PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Studies have shown that the roots, bark, flowers, leaves and fruits of Cinnamomum burmanii are rich in volatile oils, which are widely used in the food and pharmaceutical industries, and the components and proportions of volatile oils in different organs are different, but the volatile oil components in Cinnamomum cuntiflora flowers but no report

Method used

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  • Cinnamomum burmannii flower volatile oil effective component identification method
  • Cinnamomum burmannii flower volatile oil effective component identification method

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Embodiment 1

[0019] A method for identifying active ingredients in the volatile oil of Jasmine yamba, said method separates the active ingredients from Jasmine yamba by gas chromatography, and then identifies the active ingredients by mass spectrometry, said method comprising the following steps:

[0020] A. Extraction of volatile oil from Cinnamomum yamba: Take 100g of Cinnamomum yinsinum, add 300ml of water to the volatile oil extractor, control the temperature at 100°C, keep boiling, extract for 2 hours to obtain volatile oil, dissolve the volatile oil with ether, and dry it with anhydrous sodium sulfate, that is Obtain the volatile oil of Cinnamomum burmanii to be detected;

[0021] B. Gas chromatographic conditions: inject the volatile oil obtained in step A, the chromatographic column is HP-5MS 5% phenylmethylsiloxane elastic quartz capillary column, the specification is 30 m × 0. 25 mm × 0. 25 μm, enter The sample port temperature is 250 °C, the carrier gas is nitrogen, and the flow...

Embodiment 2

[0026] A method for identifying active ingredients in the volatile oil of Jasmine yamba, said method separates the active ingredients from Jasmine yamba by gas chromatography, and then identifies the active ingredients by mass spectrometry, said method comprising the following steps:

[0027] A. Extraction of volatile oil from Cinnamomum yinsinum: Take 80g of Cinnamomum syringae, add 300ml of water to the volatile oil extractor, control the temperature at 110°C, keep boiling, extract for 2 hours to obtain volatile oil, dissolve the volatile oil with ether, dry with anhydrous sodium sulfate, and obtain The volatile oil of Cinnamomum burmanii to be tested;

[0028] B. Gas chromatographic conditions: inject the volatile oil obtained in step A, the chromatographic column is HP-5MS 5% phenylmethylsiloxane elastic quartz capillary column, the specification is 30 m × 0. 25 mm × 0. 25 μm, enter The sample port temperature is 280 °C, the carrier gas is nitrogen, and the flow rate is 1 ...

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Abstract

The invention discloses a cinnamomum burmannii flower volatile oil effective component identification method, belongs to the field of drug analysis, the cinnamomum burmannii flower volatile oil effective component identification method includes the following steps: cinnamomum burmannii flower volatile oil extraction, chromatography / mass spectrometry analysis and component identification, and by cinnamomum burmannii flower effective component identification, the cinnamomum burmannii flower resource can be fully effectively used.

Description

technical field [0001] The invention belongs to the field of drug analysis, and in particular relates to the identification of active ingredients in flowers of evergreen broad-leaved trees of the lauraceae genus. Background technique [0002] Cinnamomum [ Cinnamomum burmannii (C. G. & Th. Nees) Bl.] is an evergreen broad-leaved tree of the genus Lauraceae, also known as osmanthus, gum leaf, mountain osmanthus, wild camphor tree, and small cinnamon. It is mainly distributed in Guangdong, Guangxi, Fujian, Yunnan and other provinces. Studies have shown that the roots, bark, flowers, leaves and fruits of Cinnamomum burmanii are rich in volatile oils, which are widely used in the food and pharmaceutical industries, and the components and proportions of volatile oils in different organs are different, but the volatile oil components in Cinnamomum cuntiflora flowers But no report. [0003] Yinxianghua has the functions of dispelling cold, expelling wind and dampness, detoxifying...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/02
Inventor 李炳超刘安韬白卫娜赵爱丽史冬霞陈红燕刘丽杰张丽丽
Owner SHIJIAZHUANG YILING PHARMA
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