Preparation method for sedative and dormitive silk quilt
A silk quilt, calming technology, applied in pharmaceutical formulations, household appliances, bedspreads, etc., to reduce exhaustion, emotional tension and stress, and reduce anger.
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Embodiment 1
[0031] The preparation process of the silk quilt with sedative and sleeping function mainly includes: cotton making, finishing, and quilt making. The specific process is as follows:
[0032] (1) Cotton making: Cocoon peeling, cotton opening, soaping, degumming, degreasing, dehydration, drying to obtain silk cotton
[0033] (2) Finishing: impregnating silk cotton with sedative and hypnotic treatment agent (lavender microcapsules 3.5% OWF, binder 40g / L, penetrant JFC 5g / L, liquor ratio 1:8, soaking time 30min, temperature 60°C), shake Dry, dry (80°C, 15min). Wherein, the preparation process of lavender microcapsules is as follows:
[0034] ① Preparation of oil-in-water emulsion
[0035] Dissolve lavender in methylene chloride at a mass ratio of 1:1; add 2,4 toluene diisocyanate (1.2 times the mass of lavender), polyvinyl alcohol (PVA) (4.5 times the mass of lavender) to form an oil phase ; Measure 100L of distilled water, and add polyethylene glycol 400 (PEG400) (consumption...
Embodiment 2
[0042] The preparation process of the silk quilt with sedative and sleeping function mainly includes: cotton making, finishing and quilt making. The specific process is as follows:
[0043] (1) Cotton making: cocoon peeling, cotton opening, soaping, degumming, oil removal, dehydration, drying, silk cotton
[0044] (2) Finishing: silk cotton, impregnated with sedative and hypnotic treatment agent (lavender microcapsules 4.5% OWF, binder 35g / L, penetrant JFC 5g / L, bath ratio 1:10, soaking time 50min, temperature 55°C), drying Dry (90 °C, 15 min). Wherein, the preparation process of lavender microcapsules is as follows:
[0045] ① Preparation of oil-in-water emulsion
[0046] Dissolve lavender in cyclohexanone at a mass ratio of 1:1; add 2,4 toluene diisocyanate (1.5 times the mass of lavender) and polyvinyl alcohol (PVA) (5 times the mass of lavender) to form an oil phase ; Measure 100L of distilled water, and add polyethylene glycol 400 (PEG400) (consumption is 4 times that o...
Embodiment 3
[0053] The preparation process of the silk quilt with sedative and sleeping function mainly includes: cotton making, finishing and quilt making. The specific process is as follows:
[0054] (1) Cotton making: cocoon peeling, cotton opening, soaping, degumming, oil removal, dehydration, drying, silk cotton
[0055] (2) Finishing: silk cotton, impregnated with sedative and hypnotic treatment agent (lavender microcapsules 4.0% OWF, adhesive 40g / L, penetrant JFC 5g / L, liquor ratio 1:8, immersion time 40min, temperature 60°C), drying Dry (80°C, 20min). Wherein, the preparation process of lavender microcapsules is as follows:
[0056] ① Preparation of oil-in-water emulsion
[0057] Dissolve lavender in ethyl acetate at a mass ratio of 1:1; add 2,6 toluene diisocyanate (1.2 times the mass of lavender) and polyvinyl alcohol (PVA) (4.5 times the mass of lavender) to form an oil phase ; Measure 100L of distilled water, and add polyethylene glycol 400 (PEG400) (consumption is 4 times...
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