Cobalt selenide nano material and application thereof
A cobalt selenide nanometer and nanomaterial technology is applied in the fields of nanomaterial preparation and biomedicine to achieve the effects of enhancing immune function, high sensitivity, and preventing and treating iodine deficiency.
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Embodiment 1
[0028] Cobalt selenide nanomaterials (Co 9 Se 8 ) preparation
[0029] 1) Add 4 mmol of SeO 2 Added to containing 5 mmol Co(Ac) 2 4H 2 O in 20 mL benzyl alcohol, stirred vigorously at room temperature for 1 h;
[0030] 2) The obtained mixture was poured into a 25 mL reactor, and heated at 180 °C for 15 h;
[0031] 3) The precipitate obtained from the reaction was centrifuged, and then washed several times with biological water to obtain the black Co 9 Se 8 ;
[0032] 4) The obtained Co 9 Se 8 Add it into 5 mL of aqueous solution containing 1 mmol polyacrylic acid (PAA), and obtain PAA-modified water-soluble Co 9 Se 8 nanoflakes.
[0033] Income Co 9 Se 8 Atomic force microscopy (AFM) characterization results of nanomaterials can be found in figure 1 , the results of thickness measurement see figure 2 . It can be seen from the figure that the synthesized Co 9 Se 8 The nanomaterials are uniform in size, with an average diameter of about 100 nm and a thicknes...
Embodiment 2
[0035] Cobalt selenide nanomaterials (CoSe 2 ) preparation
[0036] 1) Add 5 mmol of SeO 2 Added to containing 2 mmol Co(Ac) 2 4H 2 O in 20 mL of ethylene glycol, stirred vigorously at room temperature for 1 h;
[0037] 2) The obtained mixture was poured into a 25 mL reactor, and heated at 180 °C for 20 h;
[0038] 3) The precipitate obtained from the reaction was centrifuged, and then washed several times with biological water to obtain black CoSe 2 ;
[0039] 4) The resulting CoSe 2 Add it to 5 mL of aqueous solution containing 0.8 mmol polyethyleneimine (PEI), and after ultrasonication and stirring overnight, PEI-modified water-soluble CoSe 2 nanomaterials.
Embodiment 3
[0041] Preparation of Cobalt Selenide Nanomaterials (CoSe)
[0042] 1) Add 1 mmol of SeO 2 Added to containing 1 mmol Co(Ac) 2 4H 2 In 10 mL ethylene glycol-glycerol 1:1 (v / v) mixture of O, stir vigorously at room temperature for 1 h;
[0043] 2) The obtained mixture was poured into a 25 mL reactor, and heated at 180 °C for 10 h;
[0044]3) The precipitate obtained from the reaction was centrifuged, and then washed several times with biological water to obtain black CoSe;
[0045] 4) The obtained CoSe was added to 5 mL of an aqueous solution containing 0.02 mmol of polyvinyl alcohol (PVA), and the PVA-modified water-soluble CoSe nanomaterials were obtained after ultrasonication and stirring overnight.
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