Sulfonated leather greasing agent containing fatty acid low-carbon ester and preparation method thereof
A technology of leather fatliquor and low-carbon ester, which is applied in leather impregnation, small raw hide/big raw hide/leather/fur treatment, small raw hide/large raw hide/leather skin/fur chemical treatment, etc., which can solve the low utilization rate of raw materials , Low product sulfonation rate, increased product failure rate, etc., to reduce side reactions of color deepening, improve flow state, and improve stability
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Embodiment 1
[0038] In this embodiment, a mixture of saturated fatty acid methyl esters whose R1 carbon chain is C12, saturated fatty acid methyl esters whose R1 carbon chain is C14, saturated fatty acid methyl esters whose R1 carbon chain is C16, and saturated fatty acid methyl esters whose R1 carbon chain is C18 is used as Raw materials, wherein, R1 carbon chain is C12 saturated fatty acid methyl ester accounts for 35%; R1 carbon chain is C14 saturated fatty acid methyl ester accounts for 15%; R1 carbon chain is C16 saturated fatty acid methyl ester accounts for 33%; R1 carbon chain is C18 saturated fatty acid methyl esters accounted for 17%.
[0039] (1) Sulfonation: Using gas-phase falling film sulfonation / sulfation laboratory equipment, saturated fatty acid methyl ester is transported from the raw material insulation cylinder with a set temperature of 55°C to the single pipe at a quantitative rate of 250 g / min through a delivery pump. The upper part of the reactor overflows to the inn...
Embodiment 2
[0044] The present embodiment adopts the mixture of saturated fatty acid butyl ester whose R1 carbon chain is C16 and saturated fatty acid methyl ester whose R1 carbon chain is C18 as raw material, wherein, R1 carbon chain is that the saturated fatty acid butyl ester of C16 accounts for 65%; R1 carbon chain is C18 saturated fatty acid butyl ester accounts for 35%.
[0045] (1) Sulfonation: Using gas-phase falling film sulfonation / sulfation laboratory equipment, saturated fatty acid butyl ester is transported from the raw material insulation cylinder with a set temperature of 55 °C to the single pipe at a quantitative rate of 324 g / min through a delivery pump. The upper part of the reactor overflows to the inner wall of the reactor after it is filled with the feed chamber. The feed pump uses a frequency converter to control the flow rate of saturated fatty acid butyl ester. The jacket water temperature outside the sulfonation reactor is 70°C. Liquid SO 2 After gasification, th...
Embodiment 3
[0050] This embodiment adopts the mixture of C16 saturated fatty acid isopropyl ester with R1 carbon chain and C18 saturated fatty acid isopropyl ester with R1 carbon chain as raw material, wherein, R1 carbon chain is C16 saturated fatty acid isopropyl ester accounts for 65%; R1 The isopropyl ester of saturated fatty acid with a carbon chain of C18 accounts for 35%.
[0051] (1) Sulfonation: Using gas-phase falling film type sulfonation / sulfation laboratory equipment, saturated fatty acid isopropyl ester is transported from the raw material insulation cylinder with a set temperature of 70°C to the single The upper part of the tube reactor is filled with the feed chamber and overflows to the inner wall of the reactor. The feed pump uses a frequency converter to control the flow rate of saturated fatty acid isopropyl ester. The jacket water temperature outside the sulfonation reactor is 80°C. Liquid SO 2 After gasification, the gas mass flow meter is controlled at 65 g / min, and...
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