An uncertainty detecting method in heating loss measurement of dibasic lead phosphite
A technology of dibasic lead phosphite and dibasic lead phosphate, applied in measuring devices, instruments, scientific instruments, etc.
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[0059] The invention provides a method for detecting uncertainty in the measurement of the heating loss of dibasic lead phosphite
[0060] step one, According to the method of heat reduction in HG / T 2339-2005 "Lead dibasic phosphite", weigh 10g of the sample of lead dibasic phosphite in a weighing bottle at 105°C ~ 110°C to constant weight, and move to In the oven, open the bottle cap so that the layer of the sample to be tested in the weighing bottle is at the same level as the mercury bulb of the oven thermometer, and the horizontal distance is not more than 100mm. Keep the temperature at 105°C-110°C for 1 hour, cover the bottle cap, and take out the weighing bottle. The measuring bottle was placed in a desiccator, cooled to room temperature, and weighed;
[0061] Step 2, the measured mathematical model
[0062] M(%)=
[0063] In the formula: m 0 ---Weighing bottle weight after constant weight (g);
[0064] m 1 --- Weighing bottle and sample weight before drying (...
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