Microcapsule fatty powder capable of increasing content of omega3-enriched meat egg milk and preparation method of microcapsule fatty powder
A technology of microcapsules and fat powder, which can be used in applications, animal feed, animal feed, etc. It can solve the problems of difficult absorption of omega 3, easy rancidity and oxidation, and achieve the effects of potency protection, extended shelf life, and good water solubility
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[0031] The present invention also relates to a method for preparing the above-mentioned microcapsule fat powder enriched in omega-3 meat, egg and milk, the steps of which are as follows:
[0032] Step 10. Mix starch and water to form a starch slurry, stir and heat to 30-35°C, add sodium hydroxide solution to adjust pH=8.5-9, continue stirring to activate; gradually add octenyl succinic anhydride diluted with ethanol, 1 The addition was completed in ~2 hours, and during the gradual addition process, the pH value of the reaction system was controlled to maintain at 8.2~8.8. After the addition of octenyl succinic anhydride was completed, continue to stir the reaction until the pH was stable at 8.5, and finally added dilute hydrochloric acid to neutralize To pH=6.5, heat up to 90°C to turn into starch paste;
[0033] Step 20. Put oil containing Ω3 into the oil phase tank, heat to 70-80°C, and add compound emulsifier and sodium stearoyl lactylate under stirring, keep warm at 70-80°...
Embodiment 1
[0037] Embodiment 1, the preparation that is rich in omega 3 microcapsule fat powder
[0038] Step 10: Add 20kg of cornstarch and 30kg of drinking water to form a starch slurry, stir and heat to 30-35°C, add sodium hydroxide solution (4%) to adjust the pH to 8.5-9, stir for half an hour, and gradually add octenyl amber Anhydride 0.6kg (diluted with 2.4kg of absolute ethanol or 95% ethanol), added in 1 to 2 hours, during the gradual addition, add sodium hydroxide solution (4%) to keep the pH of the reaction system = 8.2 to 8.8 as the pH decreases ; After adding octenyl succinic anhydride, continue to stir the reaction until the pH is stable at 8.5, and finally add dilute hydrochloric acid (3%) to neutralize to pH = 6.5, and heat up to 90 ° C to become starch paste.
[0039] Step 20: Put 500kg of oil containing Ω3 into the oil phase tank, heat to 70-80°C, add 13kg of compound emulsifier and 5.5kg of sodium stearoyl lactylate under stirring, keep warm at 70-80°C and stir until diss...
Embodiment 2
[0042] Example 2, feeding the fat powder rich in Ω3 microcapsules of the present invention, egg yolk DHA correspondingly increased
[0043] Test group:
[0044] A: Control group (BD: Fujian Hualong Group Longyan company laying hen feed)
[0045] B: Experimental group Ⅰ (BD+0.5% lipogenin)
[0046] C: Experimental group Ⅱ (BD+1% lipogenin)
[0047] Each group of 5 70-week-old Hy-line laying hens was fed continuously for 2 weeks. The results are shown in Table 1 below:
[0048] Table 1
[0049]
[0050] The results showed that: (1) Adding 1% fat powder rich in Ω3 microcapsules to the diet increased the egg weight by 8.8%.
[0051] (2) Adding 0.5% and 1.0% fat powder rich in omega3 microcapsules to the diet increased egg yolk DHA (or C22:6n3) to 32.2% and 59.3%, respectively.
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