A kind of production method for preparing ammonium dihydrogen phosphate by-product shallot special fertilizer
A technology of ammonium dihydrogen phosphate and its production method, which is applied in the direction of ammonium orthophosphate fertilizer, alkaline orthophosphate fertilizer, phosphate fertilizer, etc., which can solve problems such as stoppage, soil compaction, and unusable active ingredients in the filtrate, so as to increase the content of elements , good absorption rate
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Embodiment 1
[0054] A kind of production method of preparing ammonium dihydrogen phosphate by-product shallot special fertilizer provided by this embodiment mainly comprises the following steps:
[0055] 1) Phosphoric acid and carbonamide are mixed, the molar ratio of phosphoric acid and carbonamide is 1.2:1, and the temperature is raised from 80°C to 160°C at a heating rate of 3-8°C / min, stirred and reacted for 4-5h, and separated to obtain Intermediate, then add the intermediate to the ammonia solution, the molar ratio of the intermediate to the ammonia water is 1:1.4, adjust the temperature to 50-65°C, stir and react for 2-3 hours, after the reaction, carry out cooling crystallization and filtration treatment, the crystallization temperature The temperature is 30-35°C, and the filtrate is circulated and crystallized in the cooling crystallizer, and the obtained filter cake is ammonium dihydrogen phosphate product, and the component content in the filtrate is detected;
[0056] 2) add po...
Embodiment 2
[0061] A kind of production method of preparing ammonium dihydrogen phosphate by-product shallot special fertilizer provided by this embodiment mainly comprises the following steps:
[0062] 1) Phosphoric acid and carbonamide are mixed, the molar ratio of phosphoric acid and carbonamide is 1.5:1, and the temperature is raised from 80°C to 160°C at a heating rate of 3-8°C / min, stirred for 4-5h, and separated to obtain Intermediate, then add the intermediate to the ammonia solution, the molar ratio of the intermediate to the ammonia water is 1:1.2, adjust the temperature to 50-65°C, stir and react for 2-3 hours, after the reaction, carry out cooling crystallization and filtration treatment, the crystallization temperature The temperature is 30-35°C, and the filtrate is circulated and crystallized in the cooling crystallizer, and the obtained filter cake is ammonium dihydrogen phosphate product, and the component content in the filtrate is detected;
[0063] 2) add potassium hydr...
Embodiment 3
[0068] A kind of production method of preparing ammonium dihydrogen phosphate by-product shallot special fertilizer provided by this embodiment mainly comprises the following steps:
[0069] 1) Phosphoric acid and carbonamide are mixed, the molar ratio of phosphoric acid and carbonamide is 1.3:1, and the temperature is raised from 80°C to 160°C at a heating rate of 3-8°C / min, stirred and reacted for 4-5h, and separated to obtain Intermediate, then add the intermediate to the ammonia solution, the molar ratio of the intermediate to the ammonia water is 1:1.3, adjust the temperature to 50-65°C, stir and react for 2-3 hours, after the reaction, carry out cooling crystallization and filtration treatment, the crystallization temperature The temperature is 30-35°C, and the filtrate is circulated and crystallized in the cooling crystallizer, and the obtained filter cake is ammonium dihydrogen phosphate product, and the component content in the filtrate is detected;
[0070] 2) add po...
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