Production method for preparing tripotassium phosphate and by-producing special fertilizer for litchi
A technology of tripotassium phosphate and its production method, which is applied in the direction of chemical instruments and methods, applications, phosphorus compounds, etc., can solve the problems of poor purity of tripotassium phosphate products, achieve significant environmental protection value and economic benefits, reduce production costs, and significantly economical benefit effect
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Embodiment 1
[0048] A production method for preparing special fertilizer for litchi by-product of tripotassium phosphate,
[0049] (1) Preparation of intermediate slurry: Put phosphoric acid and carbonamide into a stirred reactor at a molar ratio of 1.95:1, and control the reaction temperature at 92°C, and stir for 20 minutes at a constant stirring speed of 50 r / min. Obtain intermediate slurry;
[0050] (2) Add potassium hydroxide: to step 1) prepare and obtain intermediate slurry and add potassium hydroxide, the concentration of the potassium hydroxide added is 30%, and the addition is 2 times of carbonamide addition, and control temperature of reaction is At 40°C, stir and react at a stirring speed of 35r / min for 30min to obtain tripotassium phosphate slurry;
[0051] (3) Crystallization separation: the tripotassium phosphate slurry obtained in step 2) is cooled and crystallized in a reactor, the temperature during cooling and crystallization is 30°C, and the content of nitrogen, phosph...
Embodiment 2
[0056] A production method for preparing special fertilizer for litchi by-product of tripotassium phosphate,
[0057] (1) Preparation of intermediate slurry: put phosphoric acid and carbonamide into a stirred reactor at a molar ratio of 2.05:1, and control the reaction temperature to 102°C, and stir at a constant stirring speed of 70r / min for 30min. Obtain intermediate slurry;
[0058] (2) Add potassium hydroxide: to step 1) prepare and obtain intermediate slurry and add potassium hydroxide, the concentration of the potassium hydroxide added is 30%, and the addition is 3 times of carbonamide addition, and control temperature of reaction is At 80°C, stir and react at a stirring speed of 40r / min for 60min to obtain tripotassium phosphate slurry;
[0059] (3) Crystallization separation: the tripotassium phosphate slurry obtained in step 2) is cooled and crystallized in a reactor, and the temperature during cooling and crystallization is 28° C., and the content of nitrogen, phosp...
Embodiment 3
[0064] A production method for preparing special fertilizer for litchi by-product of tripotassium phosphate,
[0065] (1) Preparation of intermediate slurry: put phosphoric acid and carbonamide into a stirred reactor at a molar ratio of 2:1, and control the reaction temperature at 98°C, and stir at a constant stirring speed of 60r / min for 25min. Obtain intermediate slurry;
[0066] (2) Add potassium hydroxide: to step 1) prepare and obtain intermediate slurry and add potassium hydroxide, the concentration of the potassium hydroxide added is 30%, and the addition is 2.5 times of carbonamide addition, and control temperature of reaction is At 60°C, stir and react at a stirring speed of 38r / min for 45min to obtain tripotassium phosphate slurry;
[0067] (3) Crystallization separation: the tripotassium phosphate slurry obtained in step 2) is cooled and crystallized in a reactor, and the temperature during cooling and crystallization is 25° C., and the content of nitrogen, phospho...
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