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Application of a Hydroxy Acid in Cigarettes

A technology of hydroxy acid and cigarettes, which is applied in the application field of hydroxy acid as a flavoring agent in cigarettes. It can solve the problems of intolerance to baking, fast and uneven release of aroma, and achieve low volatility, uniform aroma release, and The effect of good moisturizing effect

Active Publication Date: 2016-03-16
CHINA TOBACCO HUNAN INDAL CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In view of the above problems, the inventor tried to apply other esters which are suitable for use in cigarettes in accordance with the usual thinking of those skilled in the art, but found that the above-mentioned aromas still have fast and uneven release, Not resistant to baking and suction drying

Method used

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  • Application of a Hydroxy Acid in Cigarettes
  • Application of a Hydroxy Acid in Cigarettes
  • Application of a Hydroxy Acid in Cigarettes

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] 18.0 g of dihydrokiwi lactone and 40 g of 15% sodium hydroxide aqueous solution were added to a three-necked flask, and the temperature of the oil bath was controlled to reflux at about 50° C. and reacted for 4 hours. Then cool the solution to below 4°C and keep it constant, then add 100g of a 14.7% sulfuric acid solution to it, continue to stir for 1.0 hour, separate, remove the salt solution by washing with water, and dry with anhydrous sodium sulfate to obtain the target product 18.6 g.

Embodiment 2

[0028] 18.0 g of dihydrokiwi lactone and 40 g of 15% sodium hydroxide aqueous solution were added to a three-necked flask, and the temperature of the oil bath was controlled to reflux at about 70° C. for reaction for 4 hours. Then cool the solution to below 4°C and keep it constant, then add 100g of a 14.7% sulfuric acid solution to it, continue to stir for 1.0 hour, separate the liquids, remove the salt solution by washing with water, and dry with anhydrous sodium sulfate to obtain the target product 18.2 g.

Embodiment 3

[0030] 18.0g of dihydrokiwifruit lactone and 40g of 15% sodium hydroxide aqueous solution were added into a three-necked flask, and the temperature of the oil bath was controlled to reflux for reaction at about 90°C and reacted for 4 hours. Then cool the solution to below 4°C and keep it constant, then add 100g of a 14.7% sulfuric acid solution to it, continue to stir for 1.0 hour, separate the liquids, remove the salt solution by washing with water, and dry with anhydrous sodium sulfate to obtain the target product 17.5 g.

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PUM

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Abstract

The invention discloses the application of hydroxy acid in a cigarette. Dihydroactinidiolide is subjected to backflow reaction in a strong base solution. After complete reaction, the dihydroactinidiolide is cooled to the temperature below 4 DEG C, the temperature is kept constant, an acid solution is added slowly, the final pH value of the solution is kept between 6 and 6.5, and after liquid separating, washing and drying, the hydroxy acid is obtained. The hydroxy acid is used as flavouring substances to be added to the cigarette. After the flavouring substances are added into the cigarette, fragrance releasing is even and uniform during a cigarette smoking process, and the cigarette has a moisture preservation effect and baking resistance at the same time.

Description

Technical field [0001] The invention belongs to the field of cigarette flavor enhancement and moisturization, and specifically relates to the application of a hydroxy acid as a flavor enhancer in cigarettes. Background technique [0002] Flavoring agents that can be added to existing cigarettes include esters such as dihydrokiwi lactone, octahydrocoumarin, dihydrocoumarin, etc., which have unique aroma characteristics and are applied to cigarettes in the prior art It is widely used as a tobacco spice, especially in flue-cured tobacco. However, due to the overbearing aroma of octahydrocoumarin and dihydrocoumarin, and the problems of volatile and fast aroma release, such as dihydrokiwi lactone, octahydrocoumarin, and dihydrocoumarin, etc. The non-uniform suction and the problem of dry suction have always been detrimental to its effective use as a flavoring agent in tobacco. Those skilled in the art urgently need to find a flavoring agent to effectively solve the above problems. ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A24B15/28A24B3/12
Inventor 朱卓越杨华武王超李燕春刘金云李亚白邓昌健傅见山
Owner CHINA TOBACCO HUNAN INDAL CORP
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