Method for preparing core film of planar optical waveguide device

A planar optical waveguide and film technology, applied in the direction of optical waveguide light guide, light guide, optical components, etc., can solve the problems of increasing the refractive index of the core layer film, increasing the number of suspicious gas leakage points, increasing hardware costs, etc., achieving high refractive index, low Stress, effect of increasing refractive index

Inactive Publication Date: 2014-10-08
SOLOREIN TECH
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Problems solved by technology

However, since the mass flow controller (Mass Flow Controller, mass flow controller) in the PECVD equipment will limit the gas flow rate of germane within a certain range, it is impossible to continue to improve the flow rate of germane by continuously increasing the flow rate of germane. The refractive index of the core film
At present, most of the methods of adding a mass flow controller to the equipment are used to increase the gas flow rate of germane. However, adding a mass flow controller needs to increase the gas path branch of the equipment, and the increase of the gas path branch will inevitably lead to The increase of hardware cost and the emergence of problems such as the increase of suspected gas leakage points

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  • Method for preparing core film of planar optical waveguide device
  • Method for preparing core film of planar optical waveguide device
  • Method for preparing core film of planar optical waveguide device

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[0035] Based on this, the present invention provides a method for preparing a core film of a planar optical waveguide device to overcome the above-mentioned problems in the prior art, including:

[0036] The core film is formed by gas deposition of silane, nitrous oxide and germane;

[0037] Under certain temperature conditions, annealing is performed on the core film;

[0038] Wherein, when the gas flow rate of the silane is less than 175 sccm, the gas flow rate of the nitrous oxide is less than 3000 sccm, and the gas flow rate of the germane ranges from 12 sccm to 30 sccm, the relative ratio of the prepared core layer film to the cladding film The range of the refractive index difference is 0.75% to 1.5%.

[0039] The preparation method of the core layer film of the planar optical waveguide device provided by the present invention increases the ratio of germane in the mixed gas by reducing the gas flow rate of silane and nitrous oxide, thereby avoiding the mass flow control...

Embodiment 1

[0046] This embodiment provides a method for preparing a core film of a planar optical waveguide device, and its process flow chart is as follows figure 2 shown, including steps:

[0047]S201: forming a core film by gas deposition of silane, nitrous oxide and germane;

[0048] When PECVD is used to deposit the core layer film, it is necessary to dope germane gas in silane and nitrous oxide gas to form a germanium-doped silicon dioxide core layer film. Among them, this embodiment adopts SPTS Delta i2L type PECVD equipment to prepare the core film. The standard configuration of this equipment is to have a mass flow controller to control the flow rate of germane gas, and its plasma excitation energy is high frequency 13.56 MHz.

[0049] In this embodiment, under the condition that the gas flow rate of silane is less than 175 sccm, the gas flow rate of nitrous oxide is less than 3000 sccm, and the gas flow rate of germane is in the range of 12 sccm-30 sccm, a core layer with a t...

Embodiment 2

[0057] This embodiment provides a method for preparing a core film of a planar optical waveguide device, such as image 3 shown, including steps:

[0058] S301: Depositing silane with a gas flow rate of 80 sccm, nitrous oxide with a gas flow rate of 2400 sccm, and germane with a gas flow rate of 27 sccm to form a core film;

[0059] In this embodiment, the SPTS Delta i2L type PECVD equipment is used to prepare the core layer thin film. The standard configuration of this equipment is to have a mass flow controller to control the flow rate of germane gas, and its plasma excitation energy is a high-frequency 13.56 MHz.

[0060] In the present embodiment, the gas flow rate of silane is 80 sccm, the gas flow rate of nitrous oxide is 2400 sccm, and the gas flow rate of germane is 27 sccm. The parameter measurement of the obtained film performance is: the thickness of the prepared core layer film is about 6 μm, the refractive index The ratio is about 1.4688-1.4691, the uniformity of...

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Abstract

The invention provides a method for preparing a core film of a planar optical waveguide device. The method comprises the steps that the core film is formed by silane, nitrous oxide and germane gas in a deposition mode; under a certain temperature, annealing treatment is carried out on the core film. When the gas flow of the silane is smaller than 175 sccm, the gas flow of the nitrous oxide is smaller than 3000 sccm, and the gas flow of the germane gas ranges from 12 sccm to 30 sccm, and the difference between the relative index of refraction of the prepared core film and the relative index of refraction of a coating film ranges from 0.75% to 1.5%. According to the method, the proportion of germane gas in the mixed gas is increased by reducing the gas flow of the silane and the gas flow of the nitrous oxide, the limiting effect caused by a mass flow controller on the flow of the germane gas is avoided, and thus the germanium-doped silicon dioxide core film with a high refractive index and low stress is obtained without increasing the number of mass flow controllers.

Description

technical field [0001] The invention relates to the technical field of optical fiber communication, in particular to a method for preparing a core film of a planar optical waveguide device. Background technique [0002] The planar optical waveguide type thermo-optic tunable optical attenuator based on silicon substrate, because of its advantages of simple fabrication, good stability, small size, high yield, low cost and easy integration, will surely become the first choice for optical fiber communication systems. important components. [0003] Planar optical waveguide type thermo-optic tunable optical attenuator, such as figure 1 As shown, it generally consists of a substrate 1 , a lower cladding layer 2 , a core layer 3 and an upper cladding layer 4 . In order to make the refractive index of the formed core layer higher than that of the cladding layer, in the process of preparing the core layer film, germanium atoms are introduced into the pure silicon dioxide structure t...

Claims

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Application Information

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IPC IPC(8): G02B6/13G02B6/132
Inventor 刘春梅李朝阳
Owner SOLOREIN TECH
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