Quick drying acrylate polymer and preparation method thereof
A technology of acrylate and methyl methacrylate, which is applied in the field of quick-drying acrylate polymer and its preparation, can solve the problems that the analytical ability cannot meet the product requirements, the vacuum is not good, and the industrialization promotion cannot be carried out. Excellent photosensitivity and resolution, excellent non-stickiness, and the effect of meeting the requirements of high-precision circuit etching
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[0060] (1), add 360g o-cresol novolak epoxy resin, 125g acrylic acid, 2.5g as triphenylphosphine, 450g propylene glycol methyl ether acetate in the 2L detachable flask that possesses thermometer, reflux condenser, stirrer As a solvent, heat up to 115°C for 12 hours, then cool to 60°C, add 250g of phthalic anhydride and 0.8g of p-methoxyphenol as a polymerization inhibitor, heat up to 100°C for 8 hours, then cool down to Add 100 g of glycidyl methacrylate and 0.6 g of hydroquinone as a polymerization inhibitor after 60 ° C, and control the temperature at 95 ° C for 8 hours to obtain a quick-drying carboxyl-containing photosensitive resin of the present invention; The fast-drying carboxyl group-containing photosensitive resin has a solid content of 65wt%, an acid value of 55-65 mgKOH / g, and an average molecular weight of 10,000;
[0061] (2) Add 90g of acrylic acid, 480g of propylene glycol methyl ether acetate into a 2L detachable flask equipped with a thermometer, a reflux con...
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