Simple and quick detection method for residual quinclorac in soil

The technology of a quinclorac and detection method is applied in the field of simple and rapid detection of soil residual quinclorac, which can solve the problems of high detection cost, few farmers actively adopting it, and passive detection without much meaning, so as to be easy to popularize and apply , strong operability, easy to learn and use

Active Publication Date: 2013-05-22
PLANT PROTECTION RES INST OF GUANGDONG ACADEMY OF AGRI SCI
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Problems solved by technology

[0004] At present, the detection method of quinclorac soil residue mainly adopts high-performance liquid chromatography with ultraviolet spectrophotometric detector and mass spectrometer to measure both at home and abroad, and there are also enzyme-linked immunosorbent assays currently under study. These The analysis and determination methods all require expensive instruments and reagents, as well as complex soil sample pretreatment, which cannot be operated by ordinary personnel. Its advantage is high accuracy, and it is mainly used in the research of the degradation of herbicide residues; and for For farmers, the above-mentioned method is not only expensive to use, but also needs to find a unit with corresponding testing qualifications, so farmers seldom adopt it on their own initiative; and once the residual pesticide damage occurs, the soil samples are taken for the above-mentioned detection and diagnosis, and the loss has already been lost. Irreversible, and later passive detection is meaningless

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Embodiment Construction

[0012] Sensitive indicator plants were screened, and tobacco, tomato, eggplant, pepper and celery, which were sensitive to the herbicide quinclorac, were selected for comparison, and a series of doses of poisonous soil (0, 9.4× 10 -4 , 1.9×10 -3 , 3.8×10 -3 , 7.6×10 -3 , 1.5×10 -2 , 3.0×10 -2 , 6.0×10 -2 mg / Kg), nightshade at 3.8×10 -3 mg / Kg quinclorac soil residues showed symptoms of growth inhibition and deformity, other vegetable crops in 7.6 × 10 -3 mg / Kg showed growth inhibition, so the test results showed that nightshade is the most sensitive plant to quinclorac.

[0013] The present invention uses the screened Solanum nigrum for the first time as the best indicator plant for determining soil residual quinclorac. Solanum nigrum (solanum nigrum L.) is an annual herbaceous plant of the Solanaceae genus Solanaceae. It is distributed in farmland or wasteland all over my country. It is very easy to collect plants for potting to collect mature seeds or harvest seeds at...

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Abstract

The invention discloses a simple and quick detection method for residual quinclorac in soil. The method comprises the steps of: acquiring to-be-detected soil before crop rotation; and carrying out pot culturing on indicative plants, namely nightshade, alatum moench or photeinocarpum nakamura, which is sensitive to quinclorac by in the soil, and detecting and judging the safety of residual quinclorac soils on potatoes cultured in the following season. Compared with the conventional instrumental analysis and detection method, the simple and quick detection method for the residual quinclorac in the soil has the characteristics of simplicity, convenience, low cost and strong operability, is conveniently learned, handled and used by users and is suitable for carrying out determining and evaluation on the safety of the soil before the crop rotation of large-area rice and vegetables, professional staff and expensive instruments and equipment are not required, the popularization and the application are liable, and the effective basis is provided for field management of safety production.

Description

technical field [0001] The invention relates to a method for detecting pesticide residues in soil, in particular to a simple and rapid method for detecting residual soil using the herbicide quinclorac (quinclorac), which is used for detecting and evaluating previous rice crops before rice-vegetable rotation. The safety of cropping vegetables (mainly potatoes) in the soil where the herbicide quinclorac has been used in the fields. Background technique [0002] Chemical weeding is an efficient and economical weeding technology. With the continuous development of agricultural science and technology in my country, chemical herbicides are more and more widely used in agricultural production, and farmers are increasingly dependent on chemical herbicides. With the continuous expansion of chemical herbicide application amount and application area, the problem of herbicide phytotoxicity is also increasing year by year, and phytotoxicity has become an important factor affecting agricu...

Claims

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Application Information

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IPC IPC(8): G01N33/50
Inventor 冯莉田兴山岳茂峰杨彩宏崔烨高家东张泰劼张纯
Owner PLANT PROTECTION RES INST OF GUANGDONG ACADEMY OF AGRI SCI
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