Salty-reducing additive for tobaccos, and preparation method and application of salty-reducing additive
An additive and technology for cigarettes, which is applied in the field of preparation of salt-reducing additives for cigarettes, can solve the problems of reducing cigarettes, and achieve the effects of comfortable aftertaste, transparent fragrance, good market prospects and application value
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Embodiment 1
[0018] Take 100 grams of licorice and 50 grams of stevia, 150 grams in total, pass through a 200-mesh sieve after crushing, and extract with 1000 grams of 90% ethanol under reflux for 4 hours, extract twice, combine the filtrates, and concentrate under reduced pressure at a water bath temperature of 50°C to 50mL. Add 50mL of Chinese herbal medicine extract to 200g of macroporous adsorption resin HPD-100, wash with distilled water until colorless, then elute with 70% ethanol 4 times the volume of the resin, collect the eluate, and pass the eluate through the hollow fiber ultrasonography filter (polysulfone membrane, membrane molecular weight cut-off <10000 Daltons) ultrafiltration to obtain ultrafiltrate. Concentrate the ultrafiltrate under reduced pressure at a water bath temperature of 50°C to obtain 80 grams of extract. Then add 80 grams of 10% sodium acetate aqueous solution into the extract, and stir evenly to obtain the salt-reducing additive for tobacco.
[0019] Disso...
Embodiment 2
[0021] Take 200 grams of licorice and 60 grams of stevia, a total of 260 grams, crush them and sieve them, then reflux them with 2400 grams of 75% ethanol for 3 hours, extract 3 times, combine the filtrates, and concentrate under reduced pressure to 100 mL at a water bath temperature of 60 °C . Add 100mL of Chinese herbal medicine extract to 400g of macroporous adsorption resin HPD-100, wash with distilled water until colorless, then elute with 75% ethanol 5 times the volume of the resin, collect the eluate, and pass the eluate through a hollow fiber ultrasonography filter (polysulfone membrane, membrane molecular weight cut-off <10000 Daltons) ultrafiltration to obtain ultrafiltrate. The ultrafiltrate was concentrated under reduced pressure at a water bath temperature of 60° C. to obtain 162 grams of Chinese herbal medicine extract. Then add 162 grams of 10% sodium acetate aqueous solution into the extract, and stir evenly to obtain the salt-reducing additive for tobacco.
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Embodiment 3
[0024] Take 250 grams of licorice and 100 grams of stevia, a total of 350 grams, crush them, sieve them, and extract them with 3840 grams of 80% ethanol under reflux for 5 hours, extract twice, combine the filtrates, and concentrate under reduced pressure to 120 mL at a water bath temperature of 65 °C. Add 120mL of Chinese herbal medicine extract to 500g of macroporous adsorption resin HPD-100, wash with distilled water until colorless, then elute with 80% ethanol 6 times the volume of the resin, collect the eluate, and pass the eluate through a hollow fiber ultrasonography Filter (polysulfone membrane, membrane molecular weight cut-off <5000 Daltons) for ultrafiltration to obtain ultrafiltrate. The ultrafiltrate was concentrated under reduced pressure at a water bath temperature of 65° C. to obtain 198 grams of Chinese herbal medicine extract. Then add 300 grams of 10% sodium acetate aqueous solution into the extract, and stir evenly to obtain the salt-reducing additive for t...
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