Method for refining paprika red pigment
A technology for capsanthin and capsicum oleoresin, which is applied in chemical instruments and methods, azo dyes, organic dyes, etc., can solve the problems of large solvent consumption, long deodorization time, and limited industrialization implementation, and achieves simple equipment and low cost. Effect
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Embodiment 1
[0022] Add 1120 g capsicum oleoresin (color value 151.3, acetone insoluble matter 3.1%, solvent residue 2236.8 mg / kg, capsaicin 0.08%) into a 3000 mL beaker, then add 300 mL distilled water, heat and stir in a water bath at 55 °C After 2 h, 956.3 g of refined capsicum oleoresin was obtained (color value 171.4, acetone insoluble matter 0.6%, solvent residue 1327.5 mg / kg, capsaicin 0.08%). Add the refined capsicum oleoresin obtained above into a 5000 mL beaker, add 1910 g of despicing agent (the ratio of 60% ethanol to ammonia water is 4:1), stir at 35 °C for 1 h, let stand for 30 min, and then separate quickly , and then repeat despicing once more, and recover the solvent to obtain 605.4 g of capsanthin (color value 249.4). Add the obtained capsanthin into a 2000 mL retort bottle, add 630 g of distilled water, and deodorize in a water bath at 50 °C with a vacuum degree of 0.05 Mpa to 0.09 Mpa for 2 h, and finally obtain 595.7 g of high-quality capsanthin (color valence 247.1, ...
Embodiment 2
[0029] Add 1270 g capsicum oleoresin (color value 156.4, acetone insoluble matter 3.7%, solvent residue 2576.1 mg / kg, capsaicin 0.08%) into a 2000 mL beaker, then add 410 mL of distilled water, and place in a 70 °C water bath After heating and stirring for 2 h, 1100 g of refined capsicum oleoresin (color value 173.5, acetone insoluble matter 0.5%, solvent residue 1091.4 mg / kg, capsaicin 0.08%) was obtained by separation. Add the refined capsicum oleoresin obtained above into a 5000 mL beaker, add 2200 g despicing agent (the ratio of 60% ethanol to ammonia water is 5:1), stir at 40 °C for 1 h, let stand for 30 min, and then separate quickly , and then repeat despicing once more, and recover the solvent to obtain 748.3 g of capsanthin (color value 230.1). Add the capsanthin obtained above into a 3000 mL retort, add 1200 mL of distilled water, and deodorize in a water bath at 55 °C with a vacuum degree of 0.05 Mpa to 0.09 Mpa for 3 h, and finally obtain 736.3 g of high-quality ca...
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