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Method for refining paprika red pigment

A technology for capsanthin and capsicum oleoresin, which is applied in chemical instruments and methods, azo dyes, organic dyes, etc., can solve the problems of large solvent consumption, long deodorization time, and limited industrialization implementation, and achieves simple equipment and low cost. Effect

Inactive Publication Date: 2013-02-13
YUNNAN RAINBOW BIO TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Small-scale production using supercritical CO 2 Extraction deodorization, its advantage is that deodorization is thorough, as Chinese patent CN1267684A, after adding entraining agent several times, can remove peculiar smell preferably, but limit industrialization implementation with supercritical fluid technology; Chinese patent CN1272385C uses dehydrated alcohol and isopropyl The mixed solvent of alcohol is a deodorizer, which can also remove odors well, but there are problems such as large solvent consumption and long deodorization time

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Add 1120 g capsicum oleoresin (color value 151.3, acetone insoluble matter 3.1%, solvent residue 2236.8 mg / kg, capsaicin 0.08%) into a 3000 mL beaker, then add 300 mL distilled water, heat and stir in a water bath at 55 °C After 2 h, 956.3 g of refined capsicum oleoresin was obtained (color value 171.4, acetone insoluble matter 0.6%, solvent residue 1327.5 mg / kg, capsaicin 0.08%). Add the refined capsicum oleoresin obtained above into a 5000 mL beaker, add 1910 g of despicing agent (the ratio of 60% ethanol to ammonia water is 4:1), stir at 35 °C for 1 h, let stand for 30 min, and then separate quickly , and then repeat despicing once more, and recover the solvent to obtain 605.4 g of capsanthin (color value 249.4). Add the obtained capsanthin into a 2000 mL retort bottle, add 630 g of distilled water, and deodorize in a water bath at 50 °C with a vacuum degree of 0.05 Mpa to 0.09 Mpa for 2 h, and finally obtain 595.7 g of high-quality capsanthin (color valence 247.1, ...

Embodiment 2

[0029] Add 1270 g capsicum oleoresin (color value 156.4, acetone insoluble matter 3.7%, solvent residue 2576.1 mg / kg, capsaicin 0.08%) into a 2000 mL beaker, then add 410 mL of distilled water, and place in a 70 °C water bath After heating and stirring for 2 h, 1100 g of refined capsicum oleoresin (color value 173.5, acetone insoluble matter 0.5%, solvent residue 1091.4 mg / kg, capsaicin 0.08%) was obtained by separation. Add the refined capsicum oleoresin obtained above into a 5000 mL beaker, add 2200 g despicing agent (the ratio of 60% ethanol to ammonia water is 5:1), stir at 40 °C for 1 h, let stand for 30 min, and then separate quickly , and then repeat despicing once more, and recover the solvent to obtain 748.3 g of capsanthin (color value 230.1). Add the capsanthin obtained above into a 3000 mL retort, add 1200 mL of distilled water, and deodorize in a water bath at 55 °C with a vacuum degree of 0.05 Mpa to 0.09 Mpa for 3 h, and finally obtain 736.3 g of high-quality ca...

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PUM

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Abstract

The invention discloses a method for refining paprika red pigment. The method comprises the following steps of: dissolving capsicum oleoresin with distilled water; mixing ethanol with ammonia water to prepare a hot remover; adding twice quantities of hot remover into the capsicum oleoresin for stirring and separating to obtain the paprika red pigment; and adding 1-3 times of the quantity of the distilled water into the paprika red pigment to uniformly mix and deodorize for 2-3h under a vacuum condition to finish a refining process. By the method, each index of the paprika red pigment is effectively improved; a color value reaches 200-250; the capsaicine content is less than or equal to 0.005 percent; the acetone-insoluble substance content is less than or equal to 0.2 percent; and the solvent residues are less than 25 mg / kg without obvious characteristic smell. The used edulcoration agent, the hot remover and the deodorant are toxicity-free and harmless solvents, so that the method is simple in required equipment during the whole refining process, low in cost, simple in process and easy to operate, and lays a foundation for large-scale industrial production; and the exhaustion of waste gas and the drainage of waste water are substantially avoided.

Description

technical field [0001] The invention belongs to the field of natural organic chemistry, and in particular relates to a method for refining capsanthin. Background technique [0002] As colorants, natural plant pigments are widely used in industries closely related to human health, such as food processing, medicine and cosmetics. With the development of biotechnology, people pay more and more attention to the research and development of natural plant pigments, and their application prospects are very broad. [0003] Capsanthin is a natural food coloring with good safety, certain nutritional value and pharmacological effects. As early as the "Seventh Five-Year Plan" period, it was listed as one of the four natural pigments for key development by the state. In recent years, with the rise of people returning to nature, pursuing health and green consumption trends, those chemically synthesized pigments that were once widely used, despite their bright color, strong coloring power,...

Claims

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Application Information

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IPC IPC(8): C09B61/00C09B67/54
Inventor 代刚苏记欧敏功王晓云潘颉李磊
Owner YUNNAN RAINBOW BIO TECH
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