Vertical multi-stage mixing clarifying extracting device by air stirring and extracting method thereof

A technology of air agitation and extraction equipment, which is applied in the direction of solid solvent extraction, liquid solution solvent extraction, etc., to achieve continuous operation, meet industrial mass production, and avoid emulsification

Inactive Publication Date: 2014-12-24
INST OF PROCESS ENG CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0016] The purpose of the present invention is to provide an air stirring vertical multi-stage mixing clarification extraction device, which can effectively solve the problem of extraction in a short period of time, can effectively avoid emulsification, and is suitable for pharmaceutical industry, hydrometallurgy, Extraction systems that are easy to emulsify in the oil industry, food industry, etc.

Method used

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  • Vertical multi-stage mixing clarifying extracting device by air stirring and extracting method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0046] A kind of air stirring vertical multi-stage mixing clarification extraction device, such as figure 1 As shown, it is composed of 3 stages of extraction tanks stacked in series from bottom to top; each stage of extraction tank is divided into mixing tanks and clarification tanks, and the mixing tanks and clarification tanks at all levels are arranged alternately from left to right. An air agitator 7 is arranged in the mixing tank. A conduit 8 is connected to the bottom of the mixing tank, and the conduit 8 is located in the clarification tank of the previous stage. One end of the conduit 8 is connected to the bottom of the mixing tank, and an inverted cone 9 is welded at the other end. The bottom of the clarification tank is connected with a heavy phase guide pipe 10, and the heavy phase guide pipe 10 is located in the mixing tank of the previous stage.

[0047] An air outlet 6 is provided on the top of the clarification tank at the uppermost end of the device, and an a...

Embodiment 2

[0049] An air-stirred vertical multi-stage mixing and clarifying extraction device, which is composed of 30 stages of extraction tanks stacked in series from bottom to top; each stage of extraction tank is divided into a mixing tank and a clarification tank, and the mixing tank and the clarification tank Sort left and right alternately. An air agitator 7 is arranged in the mixing tank. A conduit 8 is connected to the bottom of the mixing tank, and the conduit 8 is located in the clarification tank of the previous stage. One end of the conduit 8 is connected to the bottom of the mixing tank, and an inverted cone 9 is welded at the other end. The bottom of the clarification tank is connected with a heavy phase guide pipe 10, and the heavy phase guide pipe 10 is located in the mixing tank of the previous stage.

[0050] An air outlet 6 is provided on the top of the clarification tank at the uppermost end of the device, and an air inlet 3 is provided at the bottom of the mixing t...

Embodiment 3

[0052] An air-stirred vertical multi-stage mixing and clarifying extraction device, which is composed of 15 stages of extraction tanks stacked in series from bottom to top; each stage of extraction tank is divided into mixing tank and clarification tank, and the mixing tank and clarification tank Sort left and right alternately. An air agitator 7 is arranged in the mixing tank. A conduit 8 is connected to the bottom of the mixing tank, and the conduit 8 is located in the clarification tank of the previous stage. One end of the conduit 8 is connected to the bottom of the mixing tank, and an inverted cone 9 is welded at the other end. The bottom of the clarification tank is connected with a heavy phase guide pipe 10, and the heavy phase guide pipe 10 is located in the mixing tank of the previous stage.

[0053] An air outlet 6 is provided on the top of the clarification tank at the uppermost end of the device, and an air inlet 3 is provided at the bottom of the mixing tank at t...

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Abstract

The invention discloses a vertical multi-stage mixing clarifying extracting device by air stirring. The device comprises 3-30 stages of extracting tanks which are stacked via the way of interlacing and are connected in series from bottom to top; each extracting tank is divided into a mixing tank and a clarifying tank; and the mixing tanks and the clarifying tanks are alternatively arranged left and right. An air stirrer is arranged inside the mixing tank. The extracting method comprises the steps that: firstly, air is added through an air inlet; a heavy phase enters into the mixing tank through a heavy phase inlet; a light phase enters into the mixing tank through a light phase inlet; the heavy phase is fallen and the light phase is risen; the heavy phase and the light phase are cut and smashed in the mixing tank; the cut light phase liquid drops and heavy phase liquid drops are completely mixed to be extracted; when the liquid level is higher than a clapboard; the mixing liquid of the heavy phase and the light phase enters into the clarifying tank, so that standing splitting-phase is performed; the light phase overflows into a pipe and is carried to the next-stage mixing tank by the gas; the heavy phase flows into the former-stage mixing tank; and the process is repeated, so that multi-stage extraction is finished. The extracting device is especially suitable for an easily emulsified system; and uniform mixing can be achieved under the condition of the clearness of a two-phase interface, so that the extracting process is finished.

Description

technical field [0001] The invention belongs to the technical field of extraction in chemical separation, and relates to an extraction device and an extraction method. Specifically, the invention relates to a tank-tower combined continuous extraction device and an extraction method. More specifically, the invention relates to an air-stirred A vertical multistage mixing and clarifying extraction device and an extraction method. Background technique [0002] Solvent extraction technology is a mass transfer separation process in which a liquid extractant is used to treat immiscible two-component or multi-component solutions to achieve component separation. The extraction technology can choose the appropriate extraction system and process according to the separation object and process requirements, which has the characteristics of high selectivity, good separation effect, easy operation and strong adaptability. With the wide application of extraction in atomic energy chemical i...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D11/04B01D11/02
Inventor 邢慧芳杨良嵘黄焜刘会洲
Owner INST OF PROCESS ENG CHINESE ACAD OF SCI
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