Composite decoloration adsorbent for shellfish products and preparation method of composite decoloration adsorbent
An adsorbent and product technology, which is applied in the composite decolorization adsorbent for heavy metal adsorption and its preparation, and in the field of decolorization of shellfish products, can solve the problems of great harm, great animal toxicity, and large investment in equipment, and achieve strong adsorption capacity and regeneration performance Good, good stability
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Embodiment 1
[0030] Soak attapulgite with 0.2mol / L HCl, centrifuge, dry the solid at 90°C to constant weight, roast at 300°C for 3 hours, and pass through a 200-mesh sieve to obtain acid-activated attapulgite; acid-activated attapulgite: Activated carbon powder = 1: 2 mixed evenly. Slowly dissolve chitosan with a deacetylation degree of 92% with 3.5% acetic acid solution to obtain 4% chitosan sol; mix acid-activated attapulgite with activated carbon powder, add 5% chitosan sol, and heat at 30°C Mix well to form a paste, completely wet the mixture of acid-activated attapulgite and activated carbon powder, and carry out modification reaction; then dry at 100°C to constant weight; pass through a 200-mesh sieve to obtain a composite decolorizing adsorbent.
[0031] Adsorption (use) method: add 2.5% compound decolorization adsorbent to the mussel cooking liquid to be treated at 25°C, stir and adsorb for 1 hour under natural pH conditions, centrifuge and filter with diatomaceous earth.
[0032]...
Embodiment 2
[0034] Soak attapulgite with 0.1mol / L HCl, centrifuge, dry the solid at 95°C to constant weight, roast at 350°C for 2.5h, and pass through a 200-mesh sieve to obtain acid-activated attapulgite; acid-activated attapulgite : Activated carbon powder = 1: 3 mix well. Slowly dissolve chitosan with a deacetylation degree of 90% with 4% acetic acid solution to obtain 3% chitosan sol; mix acid-activated attapulgite with activated carbon powder, add 4% chitosan sol, and heat at 25°C Mix well to form a paste, completely wet the mixture of acid-activated attapulgite and activated carbon powder, and carry out modification reaction; then dry at 95°C to constant weight; pass through a 200-mesh sieve to obtain a composite decolorizing adsorbent.
[0035] Adsorption (use) method: add 1% compound decolorization adsorbent to the mussel cooking liquid to be treated at 25°C, stir and adsorb for 1.5 hours under natural pH conditions, centrifuge and filter with diatomaceous earth.
[0036] After b...
Embodiment 3
[0038] Soak attapulgite with 0.15mol / L HCl, centrifuge, dry the solid at 85°C to constant weight, roast at 400°C for 2 hours, and pass through a 200-mesh sieve to obtain acid-activated attapulgite; acid-activated attapulgite: Activated carbon powder = 1: 2.5 and mix well. Slowly dissolve chitosan with a deacetylation degree of 85% with 3.0% acetic acid solution to obtain 3.5% chitosan sol; mix acid-activated attapulgite with activated carbon powder, add 3.5% chitosan sol, and heat at 20°C Mix well to form a paste, completely wet the mixture of acid-activated attapulgite and activated carbon powder, and carry out modification reaction; then dry at 90°C to constant weight; pass through a 200-mesh sieve to obtain a composite decolorizing adsorbent.
[0039] Adsorption (use) method: add 2.0% compound decolorizing adsorbent to the mussel cooking liquid to be treated at 20°C, stir and adsorb for 2 hours under natural pH conditions, centrifuge and filter with diatomaceous earth.
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