Coating for power lithium battery diaphragm, power lithium battery diaphragm and preparation thereof
A lithium battery diaphragm and power technology, which is applied in the field of coatings for power lithium battery diaphragms, can solve the problems of increased production costs, easy lint and powder loss of the diaphragm, etc., and achieves improved liquid absorption rate, enhanced paint leveling and water retention, Effect of improving tensile strength and cracking strength
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Embodiment 1
[0032] Containing 10% chlorinated polyvinylidene fluoride, 15% glycerol, 2.5% sodium hypochlorite, 70% N,N-dimethylformamide, 2.5% nano-silicon carbide whiskers (average diameter 50nm, length-to-diameter ratio of 50) preparation method of composite coating for power lithium battery diaphragm:
[0033] 1) Dissolve 10g of chlorinated polyvinylidene fluoride into a mixture of 15g of glycerol, 2.5g of sodium hypochlorite and 70g of N,N-dimethylformamide at a dissolution temperature of 80°C to form a viscous transparent liquid;
[0034] 2) Add 2.5g of nano-silicon carbide whiskers to the viscous transparent liquid prepared in 1), and stir at high speed until it is completely homogenized and dispersed to prepare 100g of composite coating with a viscosity of 6350mPa·s.
[0035] The preparation method of the power lithium battery separator (LSEP01): the MSEP separator in Comparative Example 1 is used as the wet-laid non-woven fabric substrate, and the composite coating can be coat...
Embodiment 2
[0038] Containing 10% chlorinated polyvinylidene fluoride, 20% glycerol, 5% sodium hypochlorite, 60% N,N-dimethylformamide, 5% nano-silicon carbide whiskers (average diameter 80nm, length-to-diameter ratio of 50) preparation method of composite coating for power lithium battery diaphragm:
[0039] 1) Dissolve 10g of chlorinated polyvinylidene fluoride into a mixture of 20g of glycerol, 5g of sodium hypochlorite and 60g of N,N-dimethylformamide at a dissolution temperature of 80°C to form a viscous transparent liquid;
[0040] 2) Add 5g of nano-silicon carbide whiskers to the viscous transparent liquid prepared in 1), and stir at a high speed until it is completely homogenized and dispersed to prepare 100g of composite coating with a viscosity of 7320mPa·s.
[0041] The preparation method of the power lithium battery separator (LSEP02): the MSEP separator in Comparative Example 1 is used as the wet-laid non-woven fabric substrate, and the composite coating can be coated on ...
Embodiment 3
[0044] Containing 15% chlorinated polyvinylidene fluoride, 20% glycerol, 2.5% sodium hypochlorite, 60% N,N-dimethylformamide, 2.5% nano-silicon carbide whiskers (average diameter 100nm, aspect ratio of 30) preparation method of composite coating for power lithium battery diaphragm:
[0045] 1) Dissolve 15g of chlorinated polyvinylidene fluoride into a mixture of 20g of glycerol, 2.5g of sodium hypochlorite and 60g of N,N-dimethylformamide at a dissolution temperature of 80°C to form a viscous transparent liquid;
[0046] 2) Add 2.5g of nano-silicon carbide whiskers to the viscous transparent liquid prepared in 1), and stir at high speed until it is completely homogenized and dispersed to prepare 100g of composite coating with a viscosity of 6410mPa·s.
[0047] The preparation method of the power lithium battery separator (LSEP03): the MSEP separator in Comparative Example 1 is used as the wet-laid non-woven fabric substrate, and the composite coating can be coated on the s...
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